Bruker VANTEC-1 Manuale utente

VÅNTEC-1

Detector

USER MANUAL

M88-E01072 5/05

BRUKER ADVANCED X-RAY SOLUTIONS

VÅNTEC-1 Detector

User Manual

BRUKER ADVANCED X-RAY SOLUTIONS

M88-E01072 5/05

ii M88-E01072 5/05

This manual covers the VÅNTEC-1 detector. To order additional copies of this publication, request the part number

shown at the bottom of the page.

East Cheryl Parkway, Madison, WI 53711. All world rights reserved.

Notice

The information in this publication is provided for reference only. All information contained in this publication is

believed to be correct and complete. Bruker AXS Inc. shall not be liable for errors contained herein, nor for inciden-

tal or consequential damages in conjunction with the furnishing, performance or use of this material. All product

specifications, as well as the information contained in this publication, are subject to change without notice.

This publication may contain or reference information and products protected by copyrights or patents and does

not convey any license under the patent rights of Bruker AXS Inc. nor the rights of others. Bruker AXS Inc. does not

assume any liabilities arising out of any infringements of patents or other rights of third parties. Bruker AXS Inc.

makes no warranty of any kind with regard to this material, including but not limited to the implied warranties of

merchantability and fitness for a particular purpose.

No part of this publication may be stored in a retrieval system, transmitted or reproduced in any way, including but

not limited to photocopy, photography, magnetic or other record without prior written permission of Bruker AXS Inc.

Address comments to: Technical Publications Department

Bruker AXS Inc.

5465 East Cheryl Parkway

Madison, Wisconsin 53711-5373

USA

All trademarks and registered trademarks are the sole property of their respective owners.

Printed in the U.S.A.

Revision Description

0 First publication.

1 Revised and expanded to contain integrated FDC information et al.

M88-E01072 v

Table of Contents

Notice . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ii

1. Safety Issues . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1

1.1 Qualified Personnel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2

1.2 Correct Usage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2

1.3 X-ray Equipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2

1.4 Hazardous Materials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-4

1.5 Proper Lifting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-4

2. Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1

3. System Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-1

3.1 The Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-2

3.1.1 Detector Cables and Connectors. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-2

3.1.2 Environmental Ratings. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-5

3.2 The Detector Controller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-5

3.2.1 Identifying Integrated and External FDC configurations . . . . . . . . . . . . . . . . . . . . . . . . . 3-5

3.3 The External Fast Diffraction Controller (FDC) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10

3.4 Detector Optics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-12

3.4.1 Beam Stop. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-14

3.4.2 Air Scatter Screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-15

3.4.3 Radial Soller Slit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-16

3.5 Counterbalance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-18

Table of Contents VÅNTEC-1 Detector User Manual

vi M88-E01072

4. Hardware Installation for the D8 ADVANCE . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1

4.1 Servicing Precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1

4.2 Shipping and Unpacking . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2

4.3 Baseline Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2

4.4 Hardware Installation (for detector controllers with an external FDC) . . . . . . . . . . . . . . . . . . . 4-3

4.4.1 Mount the Rails . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4

4.4.2 Install the Controllers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-5

4.4.3 Connect the Cable Wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-6

4.4.4 Connect the Power Supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-8

4.5 Hardware Installation (for detector controllers with an integrated FDC) . . . . . . . . . . . . . . . . . 4-8

4.5.1 Mount the Rails.. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-8

4.5.2 Connections and Cable Wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-9

4.6 Install the Network Card. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-11

4.7 Installation of the detector controller using second-generation indexer boards (AIB2G). . . . 4-12

4.7.1 Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-12

4.7.2 Connection and Cable Wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-13

4.7.3 Hardware Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-14

4.7.4 Software Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-16

4.7.5 Automated installation for AIB2G. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-16

4.7.6 Manual Installation for Theta-Theta Configuration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-17

4.7.7 Manual Installation for Theta-2Theta Configuration. . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-19

4.8 Optic Components. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-21

4.8.1 Mount the Detector Head to the

2-Theta Axis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-21

4.8.2 Mount and Align the Beam Stop . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-24

4.8.3 Mount and Align the Air Scatter Screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-26

4.8.4 Mount and Align the Radial Soller Slit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-31

5. Hardware Installation for the D4 ENDEAVOR . . . . . . . . . . . . . . . . . . . . . . . . . 5-1

5.1 Servicing Precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-1

5.2 Shipping and Unpacking . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-2

5.3 Baseline Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-2

5.4 Hardware Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-3

VÅNTEC-1 Detector User Manual Table of Contents

M88-E01072 vii

5.4.1 Mount the Rails and Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-3

5.4.2 Install the Primary Beam Stop. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-6

6. Software Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-1

6.1 Recommendations. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-1

6.2 Configuration of the Second Network Adapter “LAN 2” in the PC . . . . . . . . . . . . . . . . . . . . . . 6-2

6.3 Detector Software Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-4

6.3.1 Software Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-5

6.4 Network Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-7

6.5 Computer Port Configuration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-9

6.5.1 For detector controllers with external FDC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-9

6.5.2 For detector controllers with integrated FDC. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-9

6.5.3 Set Up Communication Parameters (both FDC types) . . . . . . . . . . . . . . . . . . . . . . . . . 6-10

6.6 Factory Default Settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-11

7. Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-1

7.1 Positional Calibration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-1

7.2 PSD Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-3

7.2.1 Create Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-3

7.2.2 Collect Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-5

7.2.3 Analyze Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-6

8. Alignment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-1

8.1 Alignment of the VÅNTEC-1 Detector and Mount . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-1

8.2 Evaluation and Data Interpretation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-4

9. Basic Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-1

9.1 VÅNTEC-1 Power-Up Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-1

9.2 VÅNTEC-1 Power-Down Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-2

9.3 Emergency Power-Down Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-3

9.4 Disconnecting the Power Plug. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-4

Table of Contents VÅNTEC-1 Detector User Manual

viii M88-E01072

9.5 Lock Out. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-4

9.6 Performing a Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-5

9.6.1 Select the Detector Type . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-5

9.6.2 Select the Scan Parameters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-6

9.6.3 Suppression of Kb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-7

9.6.4 Secondary Optics Settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-8

9.6.5 Execute an Immediate Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-8

9.7 Calculate the Optimum Secondary Slit Openings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-8

10. Preventive Maintenance and Troubleshooting . . . . . . . . . . . . . . . . . . . . . . 10-1

10.1 Cleaning the Diffraction System and Measuring Equipment . . . . . . . . . . . . . . . . . . . . . . . . 10-2

10.2 Replacing Fuses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-3

10.3 Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-4

10.4 Manual Configuration of the Controller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-6

Appendix A. Configuration Tables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .A-1

Appendix B. Spare Parts List. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-1

Appendix C. Updating the Detector Controller Firmware. . . . . . . . . . . . . . . . . .C-1

C.1 Setting up the HTTP connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . C-1

C.2 Performing the Flash Disk Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . C-4

C.3 Updating the FPGA Firmware. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . C-6

Appendix D. EC Declaration of Conformity . . . . . . . . . . . . . . . . . . . . . . . . . . . .D-1

Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Index-1

M88-E01072 1 - 1

1. Safety Issues

This manual contains notices which you should

observe to ensure your own personal safety, as

well as to protect the product and connected

equipment. These notices are highlighted in the

manual by a warning triangle and are marked as

follows according to the level of danger:

The word “Warning” indicates that death, severe

personal injury or substantial property damage

can result if proper precautions are not taken.

The word “Caution” indicates that minor

personal injury or property damage can result if

proper precautions are not taken.

NOTE: The word “Note” draws your attention to

particularly important information on the prod-

uct, handling the product or to a particular part

of the documentation.

The symbol shown above is used whenever

high voltage is present.

Safety Issues VÅNTEC-1 Detector User Manual

1 - 2 M88-E01072

1.1 Qualified Personnel

The VÅNTEC-1 may only be set up and oper-

ated in conjunction with this manual. Only per-

sonnel authorized by Bruker AXS are allowed to

work on this equipment. All repairs, adjustments

and alignments performed on any components

of the VÅNTEC-1 must be carried out strictly in

accordance with the established safety prac-

tices and standards of the country where the

equipment is installed.

1.2 Correct Usage

This device and its components may only be

used for the applications described in this man-

ual and only in connection with devices or com-

ponents from other manufacturers which have

been approved or recommended by Bruker

AXS.

This product can only function correctly and

safely if it is transported, stored, set up and

installed correctly and operated and maintained

as recommended by Bruker AXS. Protection

provided by this equipment may be impaired if it

is used in a manner not specified by Bruker

AXS.

1.3 X-ray Equipment

X-ray equipment produces potentially harmful

radiation and can be dangerous to anyone in the

immediate vicinity unless safety precautions are

completely understood and implemented. All

persons designated to operate or perform

maintenance need to be fully trained on the

nature of radiation, X-ray generating equipment

and radiation safety. All users of the X-ray

equipment are required to accurately monitor X-

ray exposure by proper use of X-ray dosimeters.

For safety issues related to the operation and

maintenance of your particular X-ray generator,

diffractometer and shield enclosure, please refer

to the manufacturer operation manuals or your

Radiation Protection Supervisor. The user is

responsible for compliance with local safety reg-

ulations.

Voltage Danger—Before installing or

servicing the detector, switch off the system to

avoid high voltage.

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