Buchi V-600 Manuale utente
Vacuum Pump V-600
Operation Manual
11593885A en
Imprint
Product Identification:
Operation Manual (Original) Vacuum Pump V-600
11593885
Publication date: 05.2016
BÜCHI Labortechnik AG
Meierseggstrasse 40
Postfach
CH-9230 Flawil 1
E-Mail: [email protected]
BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experi-
ence, especially with respect to structure, illustrations and technical detail.
This manual is copyrighted. Information from it may not be reproduced, distributed, or used for competi-
tive purposes, nor made available to third parties. The manufacture of any component with the aid of this
manual without prior written agreement is also prohibited.
BÜCHI Labortechnik AG Contents
Operation Manual Vacuum Pump V-600 iii
Contents
1 About this document...........................................................................................................6
1.1 Warning notices in this document........................................................................................................ 6
1.2 Symbols............................................................................................................................................... 6
1.2.1 Warning symbols .....................................................................................................................6
1.2.2 Mandatory directive symbols ...................................................................................................7
1.2.3 Other symbols..........................................................................................................................7
1.3 Available languages............................................................................................................................. 7
1.4 Trademarks.......................................................................................................................................... 7
2 Safety....................................................................................................................................8
2.1 Intended use........................................................................................................................................ 8
2.2 Use other than that intended ............................................................................................................... 8
2.3 Staff qualification ................................................................................................................................. 8
2.4 Residual risks ...................................................................................................................................... 9
2.4.1 Dangerous vapors.................................................................................................................... 9
2.4.2 Faults during operation ............................................................................................................9
2.4.3 Hot surfaces.............................................................................................................................9
2.5 Personal protective equipment .......................................................................................................... 10
2.6 Modifications...................................................................................................................................... 10
3 Product description...........................................................................................................11
3.1 Description of function ....................................................................................................................... 11
3.2 Configuration ..................................................................................................................................... 11
3.2.1 Front view ..............................................................................................................................11
3.2.2 Rear view ...............................................................................................................................12
3.2.3 Connections ........................................................................................................................... 13
3.2.4 Internal view...........................................................................................................................15
3.2.5 Type plate ..............................................................................................................................16
3.3 Specifications supplied ...................................................................................................................... 16
3.4 Technical data ................................................................................................................................... 17
3.4.1 Vacuum Pump V-600.............................................................................................................17
3.4.2 Ambient conditions.................................................................................................................17
3.4.3 Materials ................................................................................................................................17
4 Transport and storage ......................................................................................................18
4.1 Transport ........................................................................................................................................... 18
4.2 Storage .............................................................................................................................................. 18
Contents BÜCHI Labortechnik AG
iv Operation Manual Vacuum Pump V-600
5 Installation..........................................................................................................................19
5.1 Important considerations prior to commissioning .............................................................................. 19
5.2 Installation site................................................................................................................................... 20
5.3 Securing against earthquakes ........................................................................................................... 21
5.4 Connecting laboratory equipment...................................................................................................... 22
5.5 Connecting the silencer ..................................................................................................................... 23
5.5.1 Connecting silencer directly to V-600 ....................................................................................23
5.5.2 Connecting the silencer to the outlet of the secondary condenser ........................................24
5.6 Connecting a Woulff bottle................................................................................................................. 25
5.6.1 Connecting the Vacubox via a Woulff bottle ..........................................................................25
5.7 Connecting a secondary condenser .................................................................................................. 27
5.8 Connecting a secondary cold trap ..................................................................................................... 28
5.9 Fitting an Interface I-300.................................................................................................................... 29
5.10 Fitting a VacuBox............................................................................................................................... 30
5.11 Connecting the vacuum pump to the power supply........................................................................... 31
5.12 Connecting communication cables to the V-600 ............................................................................... 32
5.13 Assembling the BUCHI distillation system......................................................................................... 33
5.13.1 Overview: setting up communication connections................................................................. 34
5.13.2 Overview: setting up coolant tubing connections...................................................................35
5.13.3 Overview: setting up vacuum tubing connections..................................................................36
5.14 Operating the Vacuum Pump V-600 with 2 Rotavapor systems........................................................ 37
6 Operation............................................................................................................................39
6.1 Operating V-600 without Interface I-300/I-300 Pro............................................................................ 39
6.2 Operating V-600 with Interface I-300/I-300 Pro................................................................................. 39
7 Cleaning and servicing .....................................................................................................40
7.1 Cleaning............................................................................................................................................. 40
7.1.1 Important considerations when cleaning................................................................................ 40
7.1.2 Cleaning the pump.................................................................................................................40
7.1.3 Cleaning the casing ...............................................................................................................41
7.1.4 Cleaning glass components...................................................................................................41
7.1.5 Cleaning internal pump tubing ...............................................................................................41
7.1.6 Cleaning the diaphragm.........................................................................................................42
7.2 Servicing............................................................................................................................................ 42
7.2.1 Notes on servicing .................................................................................................................42
7.2.2 Dismantling and reassembling pump head............................................................................43
7.2.3 Replacing the diaphragm....................................................................................................... 47
7.2.4 Replacing the non-return valve.............................................................................................. 48
7.2.5 Replacing connecting tubes...................................................................................................50
7.2.6 Replacing O-rings ..................................................................................................................53
7.2.7 Removing non-return valve from elbow connector ................................................................54
7.2.8 Fitting GL14 union nut with tube seal..................................................................................... 55
8 Help with faults ..................................................................................................................56
8.1 Faults, possible causes and remedies............................................................................................... 56
8.2 Customer service............................................................................................................................... 57
9 Taking out of service and disposal..................................................................................58
9.1 Taking out of service.......................................................................................................................... 58
9.2 Disposal............................................................................................................................................. 58
BÜCHI Labortechnik AG Contents
Operation Manual Vacuum Pump V-600 v
10 Appendix ............................................................................................................................59
10.1 Solvent table...................................................................................................................................... 59
10.2 Spare parts and accessories ............................................................................................................. 61
10.3 Health and safety approval................................................................................................................ 62
10.4 Health and safety............................................................................................................................... 63
1 | About this document BÜCHI Labortechnik AG
6/65 Operation Manual Vacuum Pump V-600
1 About this document
These operating instructions describe the Vacuum Pump V-600 at the time supplied.
They are an integral part of the product and contain important information that is nec-
essary for safe operation and maintenance.
These operating instructions apply to all variants of the Vacuum Pump V-600 and are
intended primarily for laboratory staff.
uTo ensure safe and trouble-free operation, read these operating instructions be-
fore starting up the device and follow the guidance they contain.
uKeep the operating instructions somewhere near to the device.
uPass on the operating instructions to any subsequent owner or user.
BÜCHI Labortechnik AG accepts no liability whatsoever for any faults or damage that
result from the failure to follow these operating instructions.
uIf you still have any questions after reading these operating instructions, please
contact BÜCHI Labortechnik AG Customer Service. Contact details for your local
agents can be found on the back cover of these operating instructions or on the In-
ternet at http://www.buchi.com.
1.1 Warning notices in this document
Warning notices warn you of dangers that can occur when handling the device. There
are four danger levels, each identifiable by the signal word used.
Signal word Meaning
DANGER Indicates a danger with a high level of risk which could result in
death or serious injury if not prevented.
WARNING Indicates a danger with a medium level of risk which could result in
death or serious injury if not prevented.
CAUTION Indicates a danger with a low level of risk which could result in mi-
nor or medium-severity injury if not prevented.
IMPORTANT Indicates a danger that could result in damage to property.
1.2 Symbols
The following symbols may be displayed in this instruction manual or on the device:
1.2.1 Warning symbols
Symbol Meaning Symbol Meaning
General warning Corrosive substance
Dangerous electrical voltage Flammable substance
Biological hazard Potentially explosive atmos-
phere
Breakable items Dangerous gases
BÜCHI Labortechnik AG About this document | 1
Operation Manual Vacuum Pump V-600 7/65
Symbol Meaning Symbol Meaning
Hot surface Health-harming or irritant
substances
Risk of hand injury Strong magnetism
1.2.2 Mandatory directive symbols
Symbol Meaning Symbol Meaning
Wear safety goggles Wear protective clothing
Wear protective gloves Heavy load, do not lift with-
out assistance
1.2.3 Other symbols
NOTE
This symbol draws attention to useful and important information.
RThis character draws attention to a requirement that must be met before the in-
structions below are carried out.
uThis character indicates an instruction that must be carried out by the user.
5This character indicates the result of a correctly carried out instruction.
1.3 Available languages
These operating instructions were originally produced in German and have been
translated into several other languages. The translations are available on the en-
closed CD or can be obtained as a PDF file via http://www.buchi.com.
1.4 Trademarks
Product names and registered or unregistered trademarks that are used in this in-
struction manual are used only for identification and remain the property of the owner
in each case.
For example, Rotavapor® is a registered trademark of BÜCHI Labortechnik AG.
2 | Safety BÜCHI Labortechnik AG
8/65 Operation Manual Vacuum Pump V-600
2 Safety
2.1 Intended use
The Vacuum Pump V-600 has been designed and built as an item of laboratory
equipment. Its intended use is the evacuation of laboratory apparatus. This is done by
means of a PTFE-diaphragm pump – with or without regulation by a vacuum con-
troller.
PTFE-diaphragm pumps are used primarily for the following applications:
Evacuating distillation apparatus, in particular rotary evaporators (Rotavapor®)
Vacuum filtration
Vacuum-drying cabinets
Drying kilns
2.2 Use other than that intended
Use of any kind other than that referred to and any application that does not comply
with the technical specifications constitutes use other than that intended. The opera-
tor alone is liable for any damage brought about by use of the device in a manner
other than that intended.
In particular, the following applications are not permissible:
Use in areas which require explosion-safe apparatus.
Pumping of liquids and solid particles.
Processing samples which could be caused to explode or ignite by impact, friction,
heat or sparks (e.g. explosives).
Use for analysis (e.g. Kjeldahl).
Generation of positive pressure (pressurizing a system).
Operation at ambient temperatures >40 °C.
2.3 Staff qualification
Unqualified persons are unable to identify risks and are therefore exposed to greater
dangers.
The device may only be operated by suitably qualified laboratory staff.
These operating instructions are aimed at the following target groups:
Users
Users are persons that meet the following criteria:
They have been instructed in the use of the device.
They are familiar with the contents of these operating instructions and the applica-
ble safety regulations and apply them.
They are able on the basis of their training or professional experience to assess
the risks associated with the use of the device.
BÜCHI Labortechnik AG Safety | 2
Operation Manual Vacuum Pump V-600 9/65
Operator
The operator (generally the laboratory manager) is responsible for the following as-
pects:
The device must be correctly installed, commissioned, operated and serviced.
Only suitably qualified staff may be assigned the task of performing the operations
described in these operating instructions.
The staff must comply with the locally applicable requirements and regulations for
safe and hazard-conscious working practices.
Safety-related incidents that occur while using the device should be reported to the
manufacturer ([email protected]).
BUCHI service technicians
Service technicians authorized by BUCHI have attended special training courses and
are authorized by BÜCHI Labortechnik AG to carry out special servicing and repair
measures.
2.4 Residual risks
The device has been developed and manufactured using the latest technological ad-
vances. Nevertheless, risks to persons, property or the environment can arise if the
device is used incorrectly.
Appropriate warnings in this manual serve to alert the user to these residual dangers.
2.4.1 Dangerous vapors
Distillation can produce dangerous vapors that are capable of causing life-threatening
toxic effects.
uDo not inhale any vapors produced during distillation.
uEnsure that vapors are removed by a suitable fume hood.
uOnly use the device in well ventilated areas.
uIf vapors escape from joints or connections, check the seals concerned and re-
place them if necessary.
uDo not distill any unknown fluids.
uObserve the safety data sheets for all fluids used.
2.4.2 Faults during operation
If a device is damaged, sharp edges or exposed electrical wires can cause injuries.
uRegularly check device for visible damage.
uIf faults occur, switch off the device immediately, unplug the power cord and in-
form the operator.
uDo not continue to use devices that are damaged.
2.4.3 Hot surfaces
The surfaces of the device can become very hot. If touched they can cause skin
burns.
uDo not touch hot surfaces or else wear suitable protective gloves.
2 | Safety BÜCHI Labortechnik AG
10/65 Operation Manual Vacuum Pump V-600
2.5 Personal protective equipment
Depending on the application, hazards due to heat and/or corrosive chemicals may
arise.
uAlways wear appropriate personal protective equipment such as safety goggles,
protective clothing and gloves.
uMake sure that the personal protective equipment meets the requirements of the
safety data sheets for all chemicals used.
2.6 Modifications
Unauthorized modifications may impair safety and lead to accidents.
uUse only genuine BUCHI accessories, spare parts and consumables.
uTechnical modifications to the device or accessories should only be carried out
with the prior written approval of BÜCHI Labortechnik AG and only by authorized
BUCHI technicians.
BUCHI accepts no liability whatsoever for damage arising as a result of unauthorized
modifications.
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