Agilent Technologies ETC 60 Manuale utente

Agilent Electrothermal Temperature Controller

ETC 60

User’s Guide

Notices

Manual Part Number

8510137200

Edition 10, August 2021

No part of this manual may be

reproduced in any form or by any

means (including electronic storage

and retrieval or translation into a

foreign language) without prior

agreement and written consent from

Agilent Technologies, Inc. as governed

by United States and international

Agilent Technologies, Australia (M) Pty

Ltd

679 Springvale Road

Mulgrave, Victoria, 3170

Australia

www.agilent.com

Printed in Malaysia

Warranty

The material contained in this

document is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further, to

the maximum extent permitted by

applicable law, Agilent disclaims all

warranties, either express or implied,

with regard to this manual and any

information contained herein,

including but not limited to the implied

warranties of merchantability and

fitness for a particular purpose.

Agilent shall not be liable for errors or

for incidental or consequential

damages in connection with the

furnishing, use, or performance of this

document or of any information

contained herein. Should Agilent and

the user have a separate written

agreement with warranty terms

covering the material in this document

that conflict with these terms, the

warranty terms in the separate

agreement shall control.

Technology Licenses

The hardware and/or software

described in this document are

furnished under a license and may be

used or copied only in accordance with

the terms of such license.

Restricted Rights Legend

U.S. Government Restricted Rights.

Software and technical data rights

granted to the federal government

include only those rights customarily

provided to end user customers.

Agilent provides this customary

commercial license in Software and

technical data pursuant to FAR 12.211

(Technical Data) and 12.212

(Computer Software) and, for the

Department of Defense, DFARS

252.227-7015 (Technical Data -

Commercial Items) and DFARS

227.7202-3 (Rights in Commercial

Computer Software or Computer

Software Documentation).

Safety Notices

A CAUTION notice denotes a hazard. It

calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indicated

conditions are fully understood and

met.

WARNING

CAUTION

Contents

Agilent Electrothermal Temperature Controller ETC 60 User’s Guide 3

Contents

1Safety Practices and Hazards 7

Manufactured 7

Verifying Safe State 7

General 8

Hazard Warnings 8

Electrical Hazards 8

Chemical Hazards 9

Notes and Tips 9

Warning Symbols 10

Information Symbols 10

Color Coding 11

2Getting Started 13

Introduction 13

Unpacking 14

Temperature Control Module 15

Workhead 16

Pre-Installation 17

Voltage Selector 17

Installation Overview 18

Installing the Workhead Bracket (Flame Models) 19

ETC 60 Workhead Bracket Installation on Zeeman Instruments 22

Installing the Workhead 23

Installing an Absorption Cell 26

Installing the VGA 27

Contents

Agilent Electrothermal Temperature Controller ETC 60 User’s Guide 4

3Operation 29

Power Up 30

Error on Startup 31

Making Selections 31

Common Menu Options 32

Methods 32

Predefined Isothermal Methods 32

Manual Isothermal Method 33

Manual Step Method 33

Changing Settings 34

Unattended Operation 35

Shutdown Procedure 35

4Analytical Notes 37

Arsenic 38

Mercury 38

Optimal Temperature Determination 39

5Maintenance 41

Daily Maintenance 41

Replacing the Fuse 41

Quartz Absorption Cell 42

Replacing the Absorption Cell 42

Removing the Workhead 43

6Appendices 45

Appendix A — Specifications 45

Environmental 45

Contents

Agilent Electrothermal Temperature Controller ETC 60 User’s Guide 5

Appendix B —Errors 46

Warning Messages 46

Fatal Errors 47

Appendix C — Sensitivity Test Record Sheet 48

Appendix C — Sensitivity Test Record Sheet (cont.) 49

Contents

Agilent Electrothermal Temperature Controller ETC 60 User’s Guide 6

This page is intentionally left blank.

Safety Practices and Hazards

Agilent Electrothermal Temperature Controller ETC 60 User’s Guide 7

1Safety Practices and Hazards

Manufactured 7

Verifying Safe State 7

General 8

Hazard Warnings 8

Electrical Hazards 8

Chemical Hazards 9

Notes and Tips 9

Warning Symbols 10

Information Symbols 10

Color Coding 11

Manufactured

The Electrothermal Temperature Controller (ETC) is manufactured by:

Anatech BV

Nieuwstadterweg 3

6136 KN Sittard (the Netherlands)

Verifying Safe State

The following general safety precautions must be observed during all phases of

operation, maintenance, and service of this instrument.

To ensure continued safety of the instrument after maintenance or service

procedures, verify the instrument is returned to a safe state for the user. This

includes running performance checks to verify the instruments safety systems are

functioning correctly. Check the general condition of the instrument during

operation for wear or signs of corrosion that are likely to inhibit function or safety.

Failure to comply with these precautions or with specific warnings elsewhere in this

manual violates safety standards of design, manufacture, and intended use of the

instrument. Agilent Technologies assumes no liability for the customer’s failure to

comply with these requirements.

Safety Practices and Hazards

Agilent Electrothermal Temperature Controller ETC 60 User’s Guide 8

General

Operation of the Agilent ETC 60 electrothermal temperature controller and an

atomic absorption (AA) spectrometer involves the use of an electrically heated

quartz cell, high temperatures, compressed gases, and hazardous materials,

including corrosive fluids. Unskilled, improper, or careless use of the equipment can

create fire hazards or other hazards which can cause death, serious injury to

personnel, or severe damage to equipment and property.

Appropriate safety practices have been included in this operation manual and your

spectrometer operation manual, to help you operate the equipment safely. Read all

safety practices thoroughly before attempting to operate your system.

If the equipment is used in a manner not specified by the manufacturer, the

protection provided by the equipment may be impaired.

Hazard Warnings

In addition to the hazard warnings specified in your spectrometer operation manual,

specific hazard warnings have been included in this operation manual. These

warnings state the hazard, describe how to avoid it and specify the possible

consequences of not following the instructions. Read all warnings carefully and

observe them at all times.

Electrical Hazards

The ETC 60 contains electrical circuits, devices and components operating at

dangerous voltages. Contact with these circuits, devices and components can

cause death, serious injury or painful electric shock. Covers which are retained by

screws on the ETC 60 may be opened only by an Agilent field service engineer.

The ETC 60 MUST be switched off at the power switch, and the mains cable

disconnected from the mains supply BEFORE any attempt is made to remove or

replace the cell in the workhead, or the cables connecting the workhead to the

Temperature Control Module.

Safety Practices and Hazards

Agilent Electrothermal Temperature Controller ETC 60 User’s Guide 9

Use of the wrong supply voltage, connection of the accessory to an incorrectly

wired supply outlet, or lack of proper electrical grounding can create a fire hazard or

a shock hazard which can cause death, serious injury, or serious damage to

equipment.

Always use a three-wire outlet with ground connection which is adequately rated for

the load.

The installation must comply with local, state, and national safety regulations.

Ensure that the voltage selector is correctly set for the specific mains power supply

outlet that the ETC 60 will be connected to. You must do this before connecting the

accessory.

A blown fuse should be replaced with one of the size and rating stipulated in the

text adjacent to the fuse holder. Always ensure the accessory is turned off and

disconnected from the mains supply before attempting any replacement.

Chemical Hazards

Operation of an Agilent AA spectrometer may involve the use of materials that are

corrosive or otherwise hazardous. Careless, improper or unskilled use of these

materials can cause serious personal injury or an environmental hazard.

Always ensure that laboratory safety practices governing the use, handling and

disposal of hazardous materials are strictly observed. These safety practices

should include wearing the appropriate safety clothing.

Always ensure that the sample introduction system is thoroughly flushed with

distilled water and that the contents of the drain or waste container are known and

disposed of if necessary before touching any part.

Notes and Tips

A Note or Tip message is used to give advice or additional information.

NOTE This is a note.

Safety Practices and Hazards

Agilent Electrothermal Temperature Controller ETC 60 User’s Guide 10

Warning Symbols

The following is a list of symbols that appear in conjunction with warnings in this

manual and on the ETC. The hazard they describe is also shown.

A triangular symbol indicates a warning. The meanings of the symbols that may

appear alongside warnings in the documentation or on the instrument itself are as

follows:

Corrosive liquid

Electrical shock

Eye hazard

Hot surface

Noxious gas

Sharp objects

The following symbol may be used on warning labels attached to the instrument.

When you see this symbol, refer to the relevant operation or service manual for the

correct procedure referred to by that warning label.

Information Symbols

The following symbols appear on the instrument for your information.

Mains power on

Mains power off

Fuse

Single phase alternating current

Caution, disconnect all supplies, risk of electric shock

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