Agilent Technologies 1260 Infinity II Manuale utente

Agilent Technologies

Agilent InfinityLab LC Series

1260 Infinity II

Fraction Collector

User Manual

1260 Infinity II Fraction Collector User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G1364-90030

Edition

09/2017

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

a U.S. Government prime contract or sub-

contract, Software is delivered and licensed

as “Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in

FAR 2.101(a) or as “Restricted computer

software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

lation or contract clause. Use, duplication

or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

1260 Infinity II Fraction Collector User Manual 3

In This Guide

This manual contains technical reference information about the Agilent

InfinityLab LC Series 1260 Infinity II Preparative Fraction Collector

(G1364E).

1Introduction

This chapter gives an introduction to the module and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Fraction Collector

This chapter provides information on unpacking, checking on completeness,

stack considerations and installation of the module.

4 Using the Module

This chapter explains the essential operational parameters of the module.

5 Preparing the Fraction Collector

This chapter explains the operational parameters of the module.

6 Troubleshooting and Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic

features and the different user interfaces.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 1260 Infinity II Fraction Collector User Manual

In This Guide

8 Maintenance

This chapter describes the maintenance of the module.

9 Parts for Maintenance and Repair

This chapter provides information on parts for maintenance and repair.

10 Identifying Cables

This chapter provides information on cables used with the module.

11 Hardware Information

This chapter describes the module in more detail on hardware and electronics.

12 Appendix

This chapter provides additional information on safety, legal, and web.

1260 Infinity II Fraction Collector User Manual 5

Contents

1Introduction 9

Product Description 10

Features 11

Overview of the Module 12

Fraction Collector Principle 13

Leak and Waste Handling 14

2 Site Requirements and Specifications 17

Site Requirements 18

Physical Specifications 21

Performance Specifications 22

3 Installing the Fraction Collector 25

Unpacking the module 26

Optimizing the Stack Configuration 27

Install the Module 28

Installing Capillaries 32

Flow Connections to the Fraction Collector 37

Fraction Collector Trays 39

Configure Well-plate Types 42

Transporting the Fraction Collector 46

4 Using the Module 47

Configuration and Operation of the Fraction Collector 48

Solvent Information 58

Turn on/off 60

Status Indicators 62

Agilent Local Control Modules 63

6 1260 Infinity II Fraction Collector User Manual

Contents

5 Preparing the Fraction Collector 65

Best Practices 66

Solvent Information 67

Capillary Color Coding Guide 73

Install Capillary Connections 74

Setting up the Fraction Collector with the Instrument Control Interface 77

Method Parameter Settings 82

6 Troubleshooting and Diagnostics 91

User Interfaces 92

Agilent Lab Advisor Software 93

7 Error Information 95

What Are Error Messages 97

General Error Messages 98

Module Error Messages 105

8 Maintenance 117

Introduction to Maintenance 118

Warnings and Cautions 119

Cleaning the Module 120

Overview of Maintenance 121

Replace the Inlet/Waste Tubings (Preparative) 122

Replace the Valve to Needle Tubing (Preparative) 127

Exchange the Preparative Needle Assembly 130

Exchange the Needle/Capillary Carrier Assembly (Preparative) 133

Exchange the Diverter Valve 136

Exchange the Internal Tray 139

Repair or Exchange a Funnel of the Internal Tray 141

Exchange the Leak Sensor 143

Replace the Module Firmware 146

1260 Infinity II Fraction Collector User Manual 7

Contents

9 Parts for Maintenance and Repair 147

Preparative Fraction Collector Parts 148

Diverter-Valve Assembly 152

Supported Trays for a Fraction Collector 153

List of Recommended Test Tubes 154

List of Recommended Vials and Caps 155

List of Recommended Plates and Closing Mats 160

Fraction Collector Accessory Kits 162

10 Identifying Cables 163

Cable Overview 164

Analog Cables 166

Remote Cables 168

CAN/LAN Cables 172

RS-232 Cables 173

USB 174

11 Hardware Information 175

Firmware Description 176

Electrical Connections 179

Interfaces 182

Setting the 6-bit Configuration Switch 190

Early Maintenance Feedback 194

Instrument Layout 195

12 Appendix 197

General Safety Information 198

Waste Electrical and Electronic Equipment Directive 204

Radio Interference 205

Sound Emission 206

Installation of Stainless Steel Cladded PEEK Capillaries 207

Agilent Technologies on Internet 213

8 1260 Infinity II Fraction Collector User Manual

Contents

1260 Infinity II Fraction Collector User Manual

Agilent Technologies

Introduction

Product Description 10

Product Description (G1364E) 10

Features 11

Features (G1364E) 11

Overview of the Module 12

Overview of the Preparative Fraction Collector 12

Fraction Collector Principle 13

Leak and Waste Handling 14

Leak and Waste 14

Waste Concept 15

Leak Sensor 15

This chapter gives an introduction to the module and an instrument overview.

10 1260 Infinity II Fraction Collector User Manual

Introduction

Product Description

Product Description (G1364E)

The 1260 Infinity II Preparative Fraction Collector is optimized for

laboratories performing semipreparative-scale purification of milligram to low

gram quantities with typical flow rates from 5 to 100 mL/min. This fraction

collector fits in the modular design of the InfinityLab LC Series, occupying

minimal bench space. Lowest delay volumes minimize peak dispersion and

carryover for highest purity and recovery. A wide variety of collection tubes as

well as microtiter plates are available. For high-throughput applications, up to

four fraction collectors can be clustered in a single LC system.

Figure 1 Overview of the fraction collector

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3RZHUVZLWFK

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