Agilent Technologies InfinityLab LC Series Manuale utente

1290 Infinity II

Preparative Open-Bed Fraction Collector

Agilent InfinityLab LC Series

User Manual

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual

Notices

Document Information

Document No: SD-29000163 Rev. F

EDITION 11/2019

No part of this manual may be repro-

duced in any form or by any means

(including electronic storage and retrieval

or translation into a foreign language)

without prior agreement and written con-

sent from Agilent Technologies, Inc. as

governed by United States and interna-

tional copyright laws.

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this document

is provided “as is,” and is subject to being

changed, without notice, in future edi-

tions. Further, to the maximum extent

permitted by applicable law, Agilent dis-

claims all warranties, either express or

implied, with regard to this manual and

any information contained herein, includ-

ing but not limited to the implied warran-

ties of merchantability and fitness for a

particular purpose. Agilent shall not be lia-

ble for errors or for incidental or conse-

quential damages in connection with the

furnishing, use, or performance of this

document or of any information con-

tained herein. Should Agilent and the user

have a separate written agreement with

warranty terms covering the material in

this document that conflict with these

terms, the warranty terms in the separate

agreement shall control.

Technology Licenses

The hardware and/or software described

in this document are furnished under a

license and may be used or copied only in

accordance with the terms of such

license.

Restricted Rights Legend

U.S. Government Restricted Rights. Soft-

ware and technical data rights granted to

the federal government include only

those rights customarily provided to end

user customers. Agilent provides this

customary commercial license in Soft-

ware and technical data pursuant to FAR

12.211 (Technical Data) and 12.212

(Computer Software) and, for the Depart-

ment of Defense, DFARS 252.227-7015

(Technical Data - Commercial Items) and

DFARS 227.7202-3 (Rights in Commer-

cial Computer Software or Computer

Software Documentation).

Safety Notices

CAUTION

notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in damage to the product or loss

of important data. Do not proceed

beyond a

CAUTION

notice until

the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in personal injury or death.

Do not proceed beyond a WARN-

ING notice until the indicated

conditions are fully understood

and met.

1290 Infinity II Preparative

Open-Bed Fraction Collector

User Manual

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 3

In This Guide

This manual contains technical reference information about the Agilent 1290

Infinity II Preparative Open-Bed Fraction Collector (G7159B).

1Introduction

This chapter gives an introduction to the module and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical and

performance specifications.

3 Using the Fraction Collector

This chapter explains the essential operational parameters of the module.

4 Preparing the Fraction Collector

This chapter explains the operational parameters of the module.

5Troubleshootingand Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic features

and the different user interfaces.

6ErrorInformation

This chapter describes the meaning of error messages, and provides information

on probable causes and suggested actions how to recover from error conditions.

7 Maintenance

This chapter describes the maintenance of the module.

8 Parts for Maintenance and Repair

This chapter provides information on parts for maintenance and repair.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 4

9IdentifyingCables

This chapter provides information on cables used with the module.

10 Hardware Information

This chapter describes the module in more detail on hardware and electronics.

11 Appendix

This chapter provides additional information on safety, legal, and web.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 5

Contents

1Introduction8

Intended Use 9

Product Description 10

Features 11

Overview of the Module 12

Fraction Collector Principle 13

Leak and Waste Concept 14

2 Site Requirements and Specifications 16

Site Requirements 17

Physical Specifications 22

Performance Specifications 23

3 Using the Fraction Collector 27

Warnings and Cautions 28

Solvent Information 29

Turn on/off 36

Status Indicators 37

Drawer Status Indicator 38

Exchange Drawers 39

Exchange Containers 41

Replace Inlet/Waste Tubings 43

Configuration and Operation of the Open Bed Fraction Collector 47

Prepare the Module for Transportation 61

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 6

4 Preparing the Fraction Collector 63

Best Practices 64

Capillary Color Coding Guide 65

Swage Fittings 66

Setting up the Fraction Collector with the Instrument Control Interface 68

Method Parameter Settings 74

Pooling 82

5 Troubleshooting and Diagnostics 83

User Interfaces 84

Agilent Lab Advisor Software 85

6ErrorInformation86

What Are Error Messages 87

General Error Messages 88

7 Maintenance 95

Introduction to Maintenance 96

Warnings and Cautions 97

Cleaning the Module 99

Overview of Maintenance 100

Install and Remove the Top Fume Hood 101

Clean the Leak Pan 103

Replace the Dripping Adapter for the Fraction Valve 104

Replace the Module Firmware 106

8 Parts for Maintenance and Repair 107

Supported Containers 108

List of Recommended Fraction Tubes 109

Fraction Collector Accessory Kit 110

Tubing Kits 111

Top Fume Hood Kit 115

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 7

9IdentifyingCables116

Cable Overview 117

Analog Cables 119

Remote Cables 121

CAN/LAN Cables 125

RS-232 Cables 126

USB 127

10 Hardware Information 128

Firmware Description 129

Electrical Connections 132

Interfaces 134

Setting the 6-bit Configuration Switch 141

Early Maintenance Feedback 145

Instrument Layout 146

11 Appendix 147

General Safety Information 148

Waste Electrical and Electronic Equipment (WEEE) Directive 154

Radio Interference 155

Sound Emission 156

Agilent Technologies on Internet 157

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 8

1Introduction

Intended Use 9

Product Description 10

Features 11

Overview of the Module 12

Fraction Collector Principle 13

Leak and Waste Concept 14

Leak Sensor 15

This chapter gives an introduction to the module and an instrument overview.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 9

1Introduction

Intended Use

The 1290 Infinity II Preparative Open-Bed Fraction Collector is designed to be

used in combination with other InfinityLab LC modules in a preparative-scale

HPLC system to separate and purify inorganic or organic compounds via

reversed-phase chromatography applications. The module can collect fractions

of desired volume for sample purification or for later analysis.

The product is intended to be used by professional laboratory users.

1290 Infinity II Preparative Open-Bed Fraction Collector User Manual 10

1Introduction

Product Description

The Agilent 1290 Infinity II Preparative Open-Bed Fraction Collector is the ideal

solution that automatically manages high-capacity fraction collection of purified

peaks for semi-preparative and preparative scale purification. Collect milligrams

to multi-gram quantities of sample intuitive with ease. The Agilent 1290 Infinity II

Preparative Open-Bed Fraction Collector features handling a wide variety of

collection vessels with ease and capacity of up to 5.9 L by using 150 x 25 mm (L

x OD). The containers use identification tags to automatically detect the vessel

dimensions. With a novel robotic technology, Y-, Z-, theta-axis probe functionality

minimizes sample carryover between the fractions during movements between

the vessels. The Agilent 1290 Infinity II Preparative Open-Bed Fraction Collector

is optimized for flow rates up to 200 mL/min, and can be easily integrated with

any Agilent solvent delivery module, autosampler, or detector. For

high-throughput applications, you can combine up to three fraction collectors in a

single LC system. Scale up your fraction capacity based on your demand up to a

maximum of 1296 fractions.

Figure 1 Overview of the open-bed fraction collector

Status indicator

Container

Drawer

Power switch

Altri manuali per InfinityLab LC Series

Questo manuale è adatto per i seguenti modelli

Indice

Altri manuali Agilent Technologies Attrezzature da laboratorio

Agilent Technologies

Agilent Technologies Graphite Tube Atomizer GTA 120 Manuale utente

Agilent Technologies

Agilent Technologies 83620A Manuale utente

Agilent Technologies

Agilent Technologies 5100 ICP-OES Istruzioni operative

Agilent Technologies

Agilent Technologies Turbo-V 6000 Manuale utente

Agilent Technologies

Agilent Technologies 2200 TapeStation Manuale utente

Agilent Technologies

Agilent Technologies 240 Series AA Manuale utente

Agilent Technologies

Agilent Technologies 709-DS Manuale utente

Agilent Technologies

Agilent Technologies gc/ms series Manuale utente

Agilent Technologies

Agilent Technologies 1100 Series Manuale utente

Agilent Technologies

Agilent Technologies 5100 ICP-OES Istruzioni operative

Agilent Technologies

Agilent Technologies Labware MiniHub Manuale utente

Agilent Technologies

Agilent Technologies 5DX Manuale utente

Agilent Technologies

Agilent Technologies NanoDis Manuale utente

Agilent Technologies

Agilent Technologies G1982-6700 Manuale utente

Agilent Technologies

Agilent Technologies InfinityLab LC Series Manuale utente

Agilent Technologies

Agilent Technologies 7890 Series Manuale utente

Agilent Technologies

Agilent Technologies Cary 630 FTIR Manuale utente

Agilent Technologies

Agilent Technologies 1200 series Manuale utente

Agilent Technologies

Agilent Technologies 1290 Infinity II Manuale utente

Agilent Technologies

Agilent Technologies 7500 ICP-MS Manuale utente

Agilent Technologies

Agilent Technologies 1290 Infinity II 2D-LC Solution Manuale utente

Agilent Technologies

Agilent Technologies varian 320-MS LC/MS Manuale utente

Agilent Technologies

Agilent Technologies 1260 Infinity II Manuale utente

Agilent Technologies

Agilent Technologies G6011A Quiet Cover MS Manuale utente

Manuali Attrezzature da laboratorio popolari di altre marche

Qiagen

Qiagen DML 3000 Manuale utente

Queensgate

Queensgate NANOSCAN OP400 Manuale di programmazione

Conviron

Conviron GEN1000-GE Manuale utente

Parr Instrument

Parr Instrument 4560 Manuale di istruzioni

IKA

IKA IC control Manuale utente

Integra

Integra DOSE IT Manuale utente

Endress+Hauser

Endress+Hauser Cleanfit CPA875 Manuale utente

NI PXI-5422 Manuale

Collomix

Collomix Aqix Manuale utente

SPEX SamplePrep

SPEX SamplePrep 6875 Freezer/Mill Series Manuale utente

Ocean Insight

Ocean Insight FLAME-NIR+ Manuale utente

Parker

Parker ALIGN-MG-NA Manuale utente

BD 644787 Manuale utente

DENTAURUM

DENTAURUM Compact Megaplus Manuale utente

Biuged Laboratory Instruments

Biuged Laboratory Instruments BGD 626 Manuale utente

VWR

VWR SAS Super IAQ Manuale utente

illumina

illumina MiSeqDx Manuale utente

Yamato

Yamato BM510 Manuale utente