Biotage Selekt Guida

Biotage®Selekt PM Checklist | Page 

Biotage®Selekt Preventive

Maintenance Checklist

Scope

The tasks carried out during the maintenance visit shall include

servicing the listed components and a final check which is

based on factory acceptance and qualifications tests. These two

procedures constitute a Biotage®Selekt Preventive Maintenance

(PM) Plan.

Each Preventive Maintenance visit should be completed within

two hours (per system) and the system returned to operational

status – unless of course a significant problem is identified.

During the PM visit, the system is disassembled, serviced,

re-assembled and given a performance / function test to help

ensure that it will remain in good working order for the following

year.

Preventive Maintenance is a recommended procedure by

Biotage to reduce the instrument downtime and assure reliable

operation, functionality and accuracy of your Selekt system.

Customer Responsibility

The customer should ensure that the site is prepared in agree-

ment with the guidelines provided in advance.

The checks that follow include the listed configurations

SEL-2SV, SEL-2SW, SEL-2EV, SEL-2EW

Items for the Technician to Bring

P/N Description Qty. Notes

Biotage®Selekt use PM kit P/N: 416832SP

416832SP

416424SP, SFÄR-SAMPLET-

TM1, FSUD-0443-0010,

416015SP, 413245SP

Grease, test mix

kit, Tube Column

Inlet CPL, FC

needle

Spare Parts to Carry at PM Visit

SFAR-TM1 SFÄR SAMPLE TEST KIT #1 6 Normal Phase

Chomatography

SFAR-TM1-

HMN SFÄR SAMPLE TEST KIT #2 6Reverse Phase

Chomatography

415115SP INLINE CHECK VALVE 4As needed

415950SP ACCESSORY KIT 1As needed

415599SP DEUTERIUM LAMP 1consumbale

416331SP UV CELL, WITH 1/4-28

THREAD 1As needed

416427SP COLUMN HOLDER SFÄR 5G

W. CLIP, 1 PCS. 1As needed

413774 PTFE spray 1Lubrication

416025SP VALVE SOLVENT 1As needed

416026SP VALVE, HIGH PRESSURE 1As needed

UI423 BIOTAGE®SELEKT PM

CHECKLIST 1Copy to carry

Test Tools to Carry at PM Visit

356633SP CALIBRATION KIT 1Pressure test tool

416889SP CALIBRATION ACCESSORY

TOOL KIT 1Pressure test tool

accessory

416411SP CALIBRATION TOOL 1Fraction collector

calibration pin

Customer Information System Information

Company: System Serial#:

Name: System model#:

Email: Date of last PM:

Phone: Estimate date of next PM:

Biotage®Selekt PM Checklist | Page 

PrePM Report

√PM Task Notes

Print the System Status and Statistics Report.

The statistic report can be requested prior to the visit. Use the data and run rate

in the report to determine the wear and tear parts and to predict and make pro-

active replacments during the PM.

Clean and Inspect

√PM Task Notes

Open the Selekt door/covers and remove any dust/

debris.

Turn off the system and unplug the power cord from the power source. Pay

particular attention to cooling fans. 3 fans in total plus the power supply fan.

Inspect internal connectors. Check for proper contact and placement.

Clean the display and exterior of the instrument.

Clean the QR code reader. Use a cloth to wipe.

Inspect external and internal tube connections and

ensure all fittings are tight and leak free. Look for leak evidence.

Inspect the solvent inlet filters.

If clogged, advise the customer to use sonication on the filters or how to order

and replace with new. Refer to the user manual and the Maintenance chapter.

Biotage recommendation is to replace filters every 1000 hours run time.

Inspect and test the leak detectors. If applicable.

Pump and Flow Path

System Status and Statistic Report

Valve Status (switches) S1: S2: S3: S4:

Air: BP: Waste:

Pump Strokes Above 20 Bar Strokes:

Pump Board Temp Above 50 °C Minutes:

Controller Board Temp Above 50 °C Minutes:

Pump status

OK Be aware Warning

Comments:

Biotage®Selekt PM Checklist | Page 

√PM Task Notes

Lubricate the pump screws. Refer to the Service manual for details and instructions.

Replace the tube (column inlet) Part number 416015SP.

Replace broken capillary holders if worn or broken. Part number 416427SP.

Prime solvents from all channels. Check one at a

time. Verify that no air bubbles are present. If air bubbles are visible check for leaks.

Run a Pump Pressure and Safety Test Record the result. Refer to the Pump pressure and safety test. if the test fails,

replace all four check valves (415115SP).

Perform a Gradient and Pump Performance Test

and record the result.

Fill two volumetric flasks of an equal volume of 100 ml. From the Flush and Purge

menu in the SW, dispense 100 mL at 25 mL/min at a 50:50 ratio between S1 and

S2. Collect the volume to an an empty volumetric flask from C1 or C2. Record the

result.

Gradient equation:

Pump equation:

Fraction Collector

System Status and Statistic Report

Fraction Valve Strokes Number:

X-movment (meters) Distance:

Y-movment (meters) Distance:

Frac status

OK Be aware Warning

Comments:

√PM Task Notes

Check and adjust (if necessary) the level of the

system.

Adjust (elevate) the front legs to assure that the instrument leans backwards to

avoid possible leakage to front.

Check the functionality of the RFID reader. Check all RFID’s by inserting a tray in each position.

Replace the FC needle. 413245 is the standard needle.

Check and verify that the cable moves freely and

without restrictions in all positions.

Pay particular attention to the cable to the FC valve. If the FC valve needs to

be replaced or has been replaced in the past. Make sure the cable is properly

strapped.

Check that the collect valve tubes are not caught

as the arm moves. Adjust if necessary.

(100 – S1) – 0.5

(100 – S1) + (100 – S2)

(C1 or C2 – 100) – 0.5

100

Biotage®Selekt PM Checklist | Page 

Check the ribbon cable and verify that it's not

jamming as the arm moves in the Y-direction.

Check the alignment of the X-motor as the arm

moves in the X-direction.

Verify correct belt tension and the FC movement. Adjust if necessary.

Clean and lubricate the arm. Use alcohol to clean the arm and lubricate with 413774 ONLY.

Run a Fraction Function test

Verify in Service mode that all four fraction corner positions (both X and Y position)

are correct and aligned over the proper spot. If needed calibrate using the Selekt

calibration tool. Record the result.

UV Detector

System Status and Statistic Report

Total lamp burn time (h) Time:

Last calibration date Date:

Number of ignitions Counts:

Integration Time (Gain Factor) Time (ms):

UV Detector status

OK Be aware Warning

Comments:

√PM Task Notes

Remove the UV cell and inspect for contamination

or signs of leakage. If the Cell is heavliy contaminated or dirty it will not pass calibration.

Clean the Cell by flushing it with MeOH

Refer to the user manual for cleaning guidance. Ultrasonication may be neccesary.

If the UV cells needs to be replaced advise the customer that a new calibration of

the UV cell is necessary.

Calibrate the UV Detector Record the result. If calibration fails possible causes are dirty or contaminted cell

or faulty/worn UV lamp.

Final Checks

√PM Task Notes

Run the Performance and Verification test as per

UI410, using the test mix in the PM kit. Record the

result.

Record the ratio between peak 1 and peak 2.

Biotage®Selekt PM Checklist | Page 

Literature Number: UI423

Information in this document is subject to change without notice and does not represent any commitment from Biotage. E&OE.

A list of all trademarks owned by Biotage AB is available at www.biotage.com/legal. Other product and company names mentioned

herein may be trademarks or registered trademarks and/or service marks of their respective owners, and are used only for

explanation and to the owners’ benefit, without intent to infringe.

Record Section

Gradient Test

Deviation % value

Accepted critera +/- 2%

Pass/Fail Pass Fail

Pump Pressure Test

Pressure Reading Setpoint 1 Pass Fail

Acceptance pressure reading range +/- 1 bar

Pressure Reading Setpoint 2 Pass Fail

Pressure Reading Setpoint 3 Pass Fail

Fraction Collector Function test

Calibration Performed Yes No

Pass/Fail Pass Fail

UV Detector Calibration

Pass/Fail Pass Fail

Pump Volume Test

Deviation % value

Accepted criteria +/- 2%

Pass/Fail Pass Fail

Safety Test

Pass/Fail Pass Fail

Performance and Verification Test

Ratio Accepted criteria 0.84 +/- 0.15

Pass/Fail Pass Fail

Service Review

√PM Task

Review the service and test results with customer.

Record the PM service in a logbook if applicable.

Attach the report from the Checkout test to the PM report.

Attach the compete PM report and statistic report to the the electronic WO (if applicable)

Signatures and System Information

Location:

Biotage Engineer: Date:

Customer: Date:

Altri manuali per Selekt

Questo manuale è adatto per i seguenti modelli

Indice

Altri manuali Biotage Attrezzature da laboratorio

Biotage

Biotage Extrahera LV-200 Manuale utente

Biotage

Biotage Selekt Manuale utente

Biotage

Biotage Selekt Manuale utente

Biotage

Biotage TurboVap 96 Dual Manuale utente

Biotage

Biotage TurboVap 96 Dual Manuale utente

Biotage

Biotage PhyPrep Manuale utente

Biotage

Biotage V-10 Touch Manuale utente

Biotage

Biotage VacMaster Disk Manuale utente

Biotage

Biotage VacMaster 10 Manuale utente

Biotage

Biotage Extrahera Classic Guida utente

Biotage

Biotage Extrahera LV-200 Manuale utente

Biotage

Biotage Isolera Prime Manuale utente

Biotage

Biotage Lysera Manuale utente

Biotage

Biotage V-10 Touch Manuale utente

Biotage

Biotage Lysera Manuale utente

Biotage

Biotage Turbo Vap II Manuale utente

Biotage

Biotage TurboVap LV Manuale utente

Biotage

Biotage V-10 Touch Manuale utente

Biotage

Biotage PRESSURE+ 48 Manuale utente

Biotage

Biotage Flash 400 Manuale utente

Biotage

Biotage Selekt Guida utente

Biotage

Biotage Selekt Enkel Manuale utente

Biotage

Biotage PRESSURE+ 96 Manuale utente

Biotage

Biotage V-10 Touch Guida utente

Manuali Attrezzature da laboratorio popolari di altre marche

Qiagen

Qiagen DML 3000 Manuale utente

Queensgate

Queensgate NANOSCAN OP400 Manuale di programmazione

Conviron

Conviron GEN1000-GE Manuale utente

Parr Instrument

Parr Instrument 4560 Manuale di istruzioni

IKA

IKA IC control Manuale utente

Integra

Integra DOSE IT Manuale utente

Agilent Technologies

Agilent Technologies 5800 ICP-OES Manuale utente

Endress+Hauser

Endress+Hauser Cleanfit CPA875 Manuale utente

NI PXI-5422 Manuale

Collomix

Collomix Aqix Manuale utente

SPEX SamplePrep

SPEX SamplePrep 6875 Freezer/Mill Series Manuale utente

Ocean Insight

Ocean Insight FLAME-NIR+ Manuale utente

Parker

Parker ALIGN-MG-NA Manuale utente

BD 644787 Manuale utente

DENTAURUM

DENTAURUM Compact Megaplus Manuale utente

Biuged Laboratory Instruments

Biuged Laboratory Instruments BGD 626 Manuale utente

VWR

VWR SAS Super IAQ Manuale utente

illumina

illumina MiSeqDx Manuale utente