Agilent Technologies 1260 Infinity Manuale utente

Agilent Technologies

Agilent 1260 Infinity

Thermostatted Column

Compartment

User Manual

Agilent 1260 Infinity TCC User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1316-90013

Edition

06/2010

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

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or as a “commercial item” as defined in FAR

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ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

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closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

For Research Use Only

Agilent 1260 Infinity TCC User Manual 3

In This Guide…

This manual covers the Agilent 1260 Infinity Thermostatted Column

Compartments (G1316A TCC).

1 Introduction to the Column Compartment

This chapter gives an introduction to the TCC, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information about site requirements and specifications

for the module.

3 Installing the Column Compartment

This chapter describes the installation of the thermostatted column

compartment.

4 How to optimize the Column Compartment

This chapter provides information on how to optimize the thermostatted

column compartement.

5 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7TestFunctions

This chapter describes the TCC’s built in test functions.

4 Agilent 1260 Infinity TCC User Manual

In This Guide…

8 Maintenance

This chapter describes the maintenance and repair of the TCC.

9 Parts for Maintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter provides information on cables used with the 1260 Infinity series

of HPLC modules.

11 Appendix

This chapter provides addition information on safety, legal and web.

Agilent 1260 Infinity TCC User Manual 5

Contents

1 Introduction to the Column Compartment 9

Main Features 10

System Overview 11

Column-Identification System 13

Column Switching Valve (Optional) 15

Instrument Layout 18

Electrical Connections 19

Interfaces 21

Setting the 8-bit Configuration Switch (without On-Board LAN) 27

2 Site Requirements and Specifications 33

Site Requirements 34

Physical Specifications 37

Performance Specifications 38

3 Installing the Column Compartment 39

Unpacking the Column Compartment 40

Optimizing the Stack Configuration 41

Installing the Column Compartment 46

Flow Connections of the Column Compartment 49

Placing Columns 53

4 How to optimize the Column Compartment 55

Optimizing the Performance of your Column Compartment 56

5 Troubleshooting and Diagnostics 57

Overview of the Module’s Indicators and Test Functions 58

Status Indicators 59

Available Tests depending on User Interfaces 61

Agilent Lab Advisor Software 62

6 Agilent 1260 Infinity TCC User Manual

Contents

6 Error Information 63

What Are Error Messages 64

General Error Messages 65

TCC Error Messages 70

7TestFunctions 77

Thermostat Function Test 78

Pressure Test 81

Column Thermostat Temperature Calibration 82

8 Maintenance 91

Warnings and Cautions 92

Introduction to Maintenance 94

Overview of Maintenance 95

Cleaning the Module 96

Changing Column Identification Tags 97

Replacing Head Parts of Column Switching Valve 99

Correcting Leaks 102

Replacing the Module’s Firmware 103

9 Parts for Maintenance 105

Valve Options Overview 106

Column Switching Valve 2 Position/6 Port 107

Micro Column Switching Valve 2 Position-6 Port 109

Micro Column Switching Valve 2 Position/10 Port 110

Capillary Kit Column Regeneration 111

Column Regeneration Kit 113

Accessory Kits 115

10 Identifying Cables 117

Cable Overview 118

Analog Cables 120

Remote Cables 122

BCD Cables 125

CAN/LAN Cables 127

External Contact Cable 128

Agilent 1260 Infinity TCC User Manual 7

Contents

Agilent Module to PC 129

Agilent 1200 Module to Printer 130

11 Appendix 131

Safety Symbols 132

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002/96/EC) 135

Lithium Batteries Information 136

Radio Interference 137

Sound Emission 138

Use of Solvents 139

Agilent Technologies on Internet 140

8 Agilent 1260 Infinity TCC User Manual

Contents

Agilent 1260 Infinity TCC User Manual

Agilent Technologies

Introduction to the Column

Compartment

Main Features 10

System Overview 11

Column-Identification System 13

Column Switching Valve (Optional) 15

Instrument Layout 18

Electrical Connections 19

Serial Number Information 1260 Infinity 19

Electrical Connections 19

Interfaces 21

Overview Interfaces 23

Setting the 8-bit Configuration Switch (without On-Board LAN) 27

Communication Settings for RS-232C 28

Special Settings 30

This chapter gives an introduction to the TCC, instrument overview and internal

connectors.

10 Agilent 1260 Infinity TCC User Manual

1Introduction to the Column Compartment

Main Features

The Agilent 1260 Infinity Thermostatted Column Compartment is a stackable

temperature-controlled column compartment for LC. It is used for heating and

cooling to meet extreme requirements of retention time reproducibility.

The main features are:

•Peltier heating and cooling from 10 degrees below ambient up to 80 °C with

high heating and cooling speeds for maximum application flexibility and

stability.

•Holds up to three 30 cm columns and optimized design gives minimum dead

volumes and maximum efficiency.

•Two independently programmable heat exchangers contribute volumes of

only 3 µL and 6 µL.

•Electronic column-identification module as standard for GLP

documentation of column type and major column parameters.

•Optional high-quality Rheodyne®column switching valves with ceramic

stator-face assemblies for prolonged lifetime.

For specifications, see “Performance Specifications” on page 38.

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