Agilent Technologies 1100 Series Manuale utente

Agilent 1100 Series

Diode Array and

Multiple Wavelength

Detectors

Reference Manual

Notices

2004

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or

translation into a foreign language)

without prior agreement and written

consent from Agilent Technologies, Inc. as

governed by United States and

international copyright laws.

Manual Part Number

G1315-90005

Edition

Edition 05/2004

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Software Revision

This guide is valid for A.01.xx revisions of

the Agilent 1100 Series Diode Array and

Multiple Wavelength Detectors software,

where xx refers to minor revisions of the

software that do not affect the technical

accuracy of this guide.

Warranty

The material contained in this

douet is proided as is, ad is

subject to being changed, without

notice, in future editions. Further, to

the maximum extent permitted by

applicable law, Agilent disclaims all

warranties, either express or implied,

with regard to this manual and any

information contained herein,

including but not limited to the

implied warranties of merchantability

and fitness for a particular purpose.

Agilent shall not be

liable for errors or for incidental or

consequential damages in

connection with the furnishing, use,

or performance of this document or

of any information contained herein.

Should Agilent and the user have a

separate written agreement with

warranty terms covering the

material in this document that

conflict with these terms, the

warranty terms in the separate

agreement shall control.

Technology Licenses

The hardware and/or software described

in this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

Software and technical data rights granted

to federal government customers include

only those rights customarily provided to

end user Customers of Software. Agilent

provides this customary commercial

license in Software and technical data

pursuant to

rights not conveyed under these terms, it

must negotiate with Agilent to establish

acceptable terms in a written agreement

executed by all relevant parties.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in damage to the product or

loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated

conditions are fully understood

and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING

notice until the indicated

conditions are fully understood

and met.

FAR 12.211 (Technical Data) and FAR 12.212

(Computer Software) and, for Department of

Defense purchases, DFARS 252.227-7015

1100 Series DAD and MWD Reference Manual 3

(Technical Data - Commercial Items) and

DFARS 227.7202-3 (Rights in Commercial

er Software or Computer Software

Documentation). If a federal government

or other public sector Customer has a

need for

1100 Series DAD and MWD Reference Manual

I This Guide…

This manual contains information for using your Diode Array and

Multiple Wavelength Detectors.

1Installing the Detector

How to install the detector

2How to optmize the Detector

How to opimize the detector

3Troubleshooting and Test Functions

The detector’s built-in troubleshooting and test functions

4Repairing the Detector

Instructions on how to repair the detector

5Identifying Parts and Materials

Detailed illustrations and listings for parts and materials identification

for the detector

6Introduction to the Detector

An introduction to the detector, istrument overview, theory of

operation, external communication and internal connectors 7 Control

Module Screens for Agilent 1100 DAD and MWD

This chapter is intended to introduce an operator to the screens available

for operation of the Agilent 1100 diode array detector (DAD) with the

Agilent 1100 control module.

8 Specifications

Performance specifications of the detector

Annex A Safety Information

4 1100 Series DAD and MWD Reference Manual

Contents

1Installing the Detector

Site Requirements 14

Physical Specifications 16

Unpacking the Detector 17

Damaged Packaging 17

Delivery Checklist 17

Optimizing the Stack Configuration 20

Installing the Detector 22

Flow Connections to the Detector 25

2How to optmize the Detector

Optimizing the Detector Performance 30

Optimization Overview 31

Optimizing for Sensitivity, Selectivity, Linearity and Dispersion

Flow Cell Path Length 33

Peak width (response time) 35

1100 Series DAD and MWD Reference Manual 5

Sample and Reference Wavelength and Bandwidth 36

Slit Width 39

Optimizing Spectral Acquisition (DAD only) 42

Margin for Negative Absorbance 43

Optimizing Selectivity 44

Quantifying Coeluting Peaks by Peak Suppression 44

Ratio Qualifiers for Selective Detection of Compound

Classes 46

6 1100 Series DAD and MWD Reference Manual

3 Troubleshooting and Test Functions

Oeie of the Deteto’s Idiatos ad Test Futios 50

Status Indicators 51

Power Supply Indicator 51

Detector Status Indicator 51

Error Messages 53

Timeout 54

Shutdown55

Remote Timeout 56

Synchronization Lost 57

Leak 58

Leak Sensor Open 60

Leak Sensor Short 61

Compensation Sensor

Open

Compensation Sensor

Short

Fan Failed 64

Open Cover 65

Cover Violation 66

Visible Lamp Current 67

Visible Lamp Voltage 68

Communication Error 69

Calibration Values Invalid 70

Diode Current Leakage 71

Holmium Oxide Test Failed 72

1100 Series DAD and MWD Reference Manual 7

UV Lamp Current 73

UV Lamp Voltage 74

UV Ignition Failed 75

UV Heater Current 76

New Messages with the G1315B and G1365B detectors

77 Module Type Changed 78

Illegal Value From Temperature Sensor Mounted On The

Fan

Assembly 80

Illegal Value Fo „Ai Ilet" Tepeatue Seso 81

Heater Failed 82

Heater Power At Limit 83

Wavelength Recalibration 84

Test Functions 85

Holmium Oxide Test 86

Intensity Test 88

Cell Test 90

Dark-Current Test 91

Filter Test 93

4 Repairing the Detector

Introduction into Repairing the Detector 96

Using the ESD Strap 98

Overview of the Repairing of the Detector 99

Simple Repairs 101

Exchanging a Lamp 102

8 1100 Series DAD and MWD Reference Manual

Exchanging a Flow Cell 105

Repairing the Standard or Semi-Micro Flow Cell 108

Repairing the High Pressure Flow Cell 112

Replacing Capillaries on a Standard Flow Cell 114

Replacing Capillaries on a Semi-Micro and High Pressure

Flow

Cell 119

Nano Flow Cell - Replacing or Cleaning 122

Cleaning or Exchanging the Holmium Oxide Filter

127

Correcting Leaks 130

Replacing Leak Handling System Parts 131

Cleaning or Replacing Coupling Lens Assembly

132 Cleaning or Replacing Cell Support Window

135

Exchanging Internal Parts 138

Removing the Top Cover and Foam 140

Exchanging the Detector Main Board 143

Entering the Serial Number using the Control Module

146

Entering the Serial Number using the

Agilent ChemStation 147

Exchanging the Fan (G1315A/G1365A) 148

Replacing Fan Parts (G1315B/G1365B) 150

Removing the Optical Unit (G1315A/G1365A) 154

Removing the Optical Unit (G1315B/G1365B) 156

Exchanging the Source Lens (Achromat) Assembly 158

Replacing the Holmium Oxide Filter Motor162

1100 Series DAD and MWD Reference Manual 9

Exchanging the Power Supply 164

Exchanging the Leak Sensor 167

Replacing Status Light Pipe 170

Installing the Optical Unit (G1315A/G1365A) 171

Installing the Optical Unit (G1315B/G1365B) 173

Replacing the Foam and the Top Cover 175

Assembling the Main Cover 178

Replacing the Interface Board 179

Replaig the Deteto’s Fiae 180

5 Identifying Parts and Materials

Overview of Main Assemblies 182

Optical Unit Assembly 184

Standard Flow Cell 186

Semi-Micro Flow Cell 188

High Pressure Flow Cell 190

Nano Flow Cells 192

Fan Assembly Parts 196

Holmium Oxide Filter197

Coupling Lens Assembly 198

Source Lens (Achromat) Assembly 199

Cell Support Assembly 200

Control Module 201

Sheet Metal Kit (G1315A/G1365A) 202

10 1100 Series DAD and MWD Reference Manual

Sheet Metal Kit (G1315B/G1365B) 203

Plastic Parts 204

Foam Parts 205

Power and Status Light Pipes 206

Leak Parts 207

Accessory Kit 208

Cable Overview 210

Analog Cables 212

Remote Cables 215

BCD Cables 220

Auxiliary Cable 222

CAN Cable 223

External Contact Cable 224

RS-232 Cable Kit 225

LAN Cables 226

6 Introduction to the Detector

Introduction to the Detector 228

Optical System Overview 229 Electrical

Connections 232

Instrument Layout 234

Early Maintenance Feedback (EMF) 235

EMF Counters 235

Using the EMF Counters235

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