Agilent Technologies 1260 Infinity II Manuale utente

Agilent Technologies

Agilent InfinityLab LC Series

1260 Infinity II Binary Pump

User Manual

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G7112-90000 Rev. B

Edition

08/2018

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

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either express or implied, with regard

to this manual and any information

contained herein, including but not

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merchantability and fitness for a par-

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liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

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(June 1987) or any equivalent agency regu-

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lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 3

In This Guide...

This manual covers the Agilent InfinityLab LC Series 1260 Infinity II Binary

Pump (G7112B).

1Introduction

This chapter gives an introduction to the module and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information about site requirements and specifications

for the binary pump.

3UsingthePump

This chapter explains the operational parameters of the Binary Pump.

4 Optimizing Performance

This chapter gives information on how to optimize the performance of the

Binary Pump under special operational conditions.

5 Troubleshooting and Diagnostics

Overview of the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Test Functions and Calibration

This chapter explains all test functions that are available for the binary pump.

8 Maintenance

This chapter describes the maintenance of the module.

4 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual

In This Guide...

9 Parts and Materials for Maintenance

This chapter lists all parts and tools that are required for maintenance and

simple repairs.

10 Identifying Cables

This chapter provides information on cables used with the Agilent InfinityLab

LC Series modules.

11 Hardware Information

This chapter provides detailed technical information about your binary pump.

12 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

13 Appendix

This chapter provides addition information on safety, legal and web.

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 5

Contents

1Introduction 9

Instrument and Operation 10

Overview of the Hydraulic Path 15

Leak and Waste Handling 20

2 Site Requirements and Specifications 25

Site Requirements 26

Physical Specifications 29

Performance Specifications 30

3UsingthePump 33

Magnets 34

Turn on/off 35

Status Indicators 37

Best Practices 38

Leak and Waste Handling 40

Hints for Successful Use of the Binary Pump 41

Setting up the Pump with the G4208A Instant Pilot 42

Setting up the Pump with the Instrument Control Interface 43

Solvent Information 48

Algae Growth in HPLC Systems 54

Prevent Blocking of Solvent Filters 55

Normal Phase Applications 57

4 Optimizing Performance 59

When to Use a Vacuum Degasser 60

When to Use the Active Seal Wash Option 61

When to Use the Low Volume Mixer 62

When to Remove Damper and Mixer 63

How to Optimize the Compressibility Compensation Setting 66

6 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual

Contents

5 Troubleshooting and Diagnostics 69

Overview of the Module’s Indicators and Test Functions 70

User Interfaces 72

Agilent Lab Advisor Software 73

6 Error Information 75

What Are Error Messages 77

General Error Messages 78

Module Error Messages 84

7 Test Functions and Calibration 95

(System) Pressure Test 96

Valve Test 101

Binary Pump Solvent Compressibility Calibration 103

Pump Elasticity Calibration 105

Pump Leak Rate Test 107

8 Maintenance 111

Introduction to Maintenance 112

Cautions and Warnings 113

Cleaning the Module 115

Overview of Maintenance and Simple Repairs 116

Maintenance Procedures 117

Remove and Install Doors 118

Exchange the Purge Valve Frit or the Purge Valve 120

Replace the O-Ring on the Purge Valve 123

Remove the Pump Head Assembly 125

Maintenance of a Pump Head without Seal Wash 127

Maintenance of a Pump Head with Seal Wash 130

Reinstall the Pump Head Assembly 134

Seal Wear-in Procedure 136

Exchange the Active Inlet Valve (AIV) or its Cartridge 137

Exchange the Seal Wash Cartridge 140

Replace Leak Handling System Parts 142

Exchange the Outlet Valve 144

Installation of the Solvent Selection Valve Upgrade Kit 146

Exchange the Solvent Selection Valve 148

Replacing Module Firmware 151

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 7

Contents

9 Parts and Materials for Maintenance 153

Hydraulic Path with Solvent Selection Valve 154

Hydraulic Path without Solvent Selection Valve 156

Pump Head Assembly Without Seal Wash 158

Pump Head Assembly with Seal Wash Option 160

Outlet Valve 162

Purge Valve Assembly 163

Active Inlet Valve Assembly 164

HPLC System Tool Kit 165

Active Seal Wash Option 166

Solvent Cabinet 167

Bottle Head Assembly 168

Cover Parts 169

Accessory Kit 170

10 Identifying Cables 171

Cable Overview 172

Analog Cables 174

Remote Cables 176

CAN/LAN Cables 180

RS-232 Cable Kit 181

Agilent 1200 Module to Printer 182

11 Hardware Information 183

Firmware Description 184

Electrical Connections 187

Interfaces 189

Setting the 6-bit Configuration Switch 197

Early Maintenance Feedback 201

Instrument Layout 202

12 LAN Configuration 203

What You Have to Do First 204

TCP/IP parameter configuration 205

Configuration Switches 206

Initialization Mode Selection 207

Dynamic Host Configuration Protocol (DHCP) 209

Manual Configuration 212

8 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual

Contents

13 Appendix 217

General Safety Information 218

Waste Electrical and Electronic Equipment (WEE) Directive 224

Radio Interference 225

Sound Emission 226

Agilent Technologies on the Internet 227

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual

Agilent Technologies

Introduction

Instrument and Operation 10

Introduction to the Pump 10

Principle of Operation 11

Product Description 14

Features 14

Overview of the Hydraulic Path 15

Leak and Waste Handling 20

Leak Sensor 23

Waste Concept 24

This chapter gives an introduction to the module and an instrument overview.

10 InfinityLab LC Series 1260 Infinity II Binary Pump User Manual

Introduction

Instrument and Operation

Introduction to the Pump

The binary pump comprises two identical pumps integrated into one housing.

Binary gradients are created by high-pressure mixing. A built-in degasser is

available for applications that require best flow stability, especially at low flow

rates, for maximum detector sensitivity. Pulse damper and mixer can be

bypassed for low flowrate applications or whenever a minimal transient

volume is desirable. Typical applications are high throughput methods with

fast gradients on high resolution 2.1 mm columns. The pump is capable of

delivering flow in the range of 0.1 – 5 mL/min against up to 600 bar. A solvent

selection valve (optional) allows to form binary mixtures (isocratic or

gradient) from one of two solvents per channel. Active seal wash (optional) is

available for use with concentrated buffer solutions.

Figure 1 Overview of the binary pump

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