Agilent Technologies Infinity II 1290 Manuale utente

Agilent Technologies

Agilent 1290 Infinity II

Flexible Pump

User Manual

Agilent 1290 Infinity II Flexible Pump User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G7104-90000 Rev. B

Edition

12/2014

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

or contract clause. Use, duplication or dis-

closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

Agilent 1290 Infinity II Flexible Pump User Manual 3

In This Guide...

This manual covers the Agilent 1290 Infinity II Flexible Pump (G7104A).

1 Introduction

This chapter gives an introduction to the module, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3UsingthePump

This chapter explains the operational parameters of the Agilent 1290

Infinity II Flexible Pump.

4 How to Optimize the Performance of Your Module

This chapter gives hints on how to optimize the performance or use

additional devices.

5 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Maintenance

This chapter describes the maintenance of the Agilent 1290 Infinity II

Flexible Pump.

4 Agilent 1290 Infinity II Flexible Pump User Manual

In This Guide...

8 Parts and Materials

This chapter provides information on parts for maintenance and repair.

9 Identifying Cables

This chapter provides information on cables used with the modules.

10 Hardware Information

This chapter describes the pump in more detail on hardware and

electronics.

11 LAN Configuration

This chapter provides information on connecting the module to the

controller software.

12 Appendix

This chapter provides additional information on safety, legal and web.

Agilent 1290 Infinity II Flexible Pump User Manual 5

Contents

1 Introduction 9

Product Description 10

Features 11

Operating Principle 12

Positions of the Multi Purpose Valve 14

Leak and Waste Handling 19

2 Site Requirements and Specifications 23

Site Requirements 24

Physical Specifications 27

Performance Specifications 28

3UsingthePump 31

Magnets 32

Turn on/off 33

Status Indicators 34

Best Practices 35

4 How to Optimize the Performance of Your Module 39

Delay Volume and Extra-Column Volume 40

How to Configure the Optimum Delay Volume 41

How to Achieve Higher Resolution 43

Using Solvent Calibration Tables 46

5 Troubleshooting and Diagnostics 47

User Interfaces 48

Agilent Lab Advisor Software 49

6 Error Information 51

What Are Error Messages 53

General Error Messages 54

Pump Error Messages 60

6 Agilent 1290 Infinity II Flexible Pump User Manual

Contents

7 Maintenance 79

Introduction to Maintenance 81

Warnings and Cautions 82

Overview of Maintenance 84

Cleaning the Module 85

Install Fittings and Capillaries 86

Remove and Install Doors 87

Replace the Pressure Sensor 88

Replace the Inlet Weaver 90

Replace the Inlet Valve 92

Replace the Outlet Valve 93

Remove the Jet Weaver 95

Install the Jet Weaver 97

Replace the Seal Wash Pump 99

Replace the Multi-Channel Gradient Valve (MCGV) 100

Release a Stuck Inlet Valve 102

Pump Head Procedures 104

Replace the Multi Purpose Valve 133

Replace Parts of the Multi Purpose Valve 135

Replace the High Pressure Outlet Filter or Filter Frit 136

Replace Parts of the Inline Filter 138

Replace the Module Firmware 140

Prepare the Pump Module for Transport 141

8 Parts and Materials 143

Overview of Main Assemblies 144

Flow Connections 146

Pump Head Assembly Parts 148

Primary Pump Head Parts 150

Secondary Pump Head Parts 152

Multi Purpose Valve 154

Cover Parts 155

Accessory Kit 156

Tool Kit 157

Tools 158

Agilent 1290 Infinity II Flexible Pump User Manual 7

Contents

9 Identifying Cables 161

Cable Overview 162

Analog Cables 164

Remote Cables 166

CAN/LAN Cables 170

Agilent Module to PC 171

USB Cables 172

10 Hardware Information 173

Firmware Description 174

Electrical Connections 177

Interfaces 179

Setting the 8-bit Configuration Switch 184

Early Maintenance Feedback 187

Instrument Layout 188

11 LAN Configuration 189

What You Have To Do First 190

TCP/IP Parameter Configuration 191

Configuration Switch 192

Initialization Mode Selection 193

Dynamic Host Configuration Protocol (DHCP) 197

Link Configuration Selection 200

Automatic configuration with Bootp 201

Manual Configuration 211

PC and User Interface Software Setup Setup 216

12 Appendix 219

General Safety Information 220

Waste Electrical and Electronic Equipment Directive 226

Radio Interference 227

Sound Emission 228

Agilent Technologies on Internet 229

8 Agilent 1290 Infinity II Flexible Pump User Manual

Contents

Agilent 1290 Infinity II Flexible Pump User Manual

Agilent Technologies

Introduction

Product Description 10

Features 11

Operating Principle 12

Positions of the Multi Purpose Valve 14

Leak and Waste Handling 19

Waste Concept 21

This chapter gives an introduction to the module, instrument overview and

internal connectors.

10 Agilent 1290 Infinity II Flexible Pump User Manual

1Introduction

Product Description

The Agilent 1290 Infinity II Flexible Pump improves your efficiency by

combining the performance of a high- pressure mixing UHPLC pump with

the flexibility of a low- pressure mixing UHPLC pump.

The new 1290 Infinity II LC power range has a high instrument efficiency,

allowing you to run any HPLC and UHPLC method. ISET enables you to

transfer existing methods from different instrument modules - current

Agilent systems as well as instruments from other manufacturers.

The Agilent Inlet Weaver mixer, active damping or the optional Agilent

V380 Jet Weaver mixer for additional mixing capacity achieve high

analytical efficiency.

The established multipurpose valve enhances laboratory efficiency by

adding useful functionalities, for example, mixer in/out switch, filter

backflush or automatic purge, and BlendAssist software simplifies your

workflow with accurate buffer/additive blending.

Figure 1 Overview of the Flexible Pump

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