Agilent Technologies 1260 Infinity Manuale utente

Agilent Technologies

Agilent 1260 Infinity

Binary Pump

User Manual

1260 Infinity Binary Pump User Manual

Notices

2010-2013

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1312-90015 Rev. B

Edition

11/2013

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

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Technology Licenses

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Restricted Rights Legend

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or as a “commercial item” as defined in FAR

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ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

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closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

1260 Infinity Binary Pump User Manual 3

In This Guide...

This manual covers the Agilent 1260 Infinity Binary Pump (G1312B).

1 Introduction to the Binary Pump

This chapter gives an introduction to the module and an instrument

overview.

2 Site Requirements and Specifications

This chapter provides information about site requirements and

specifications for the binary pump.

3 Installing the Pump

This chapter gives information about the preferred stack setup for your

system and the installation of your binary pump.

4UsingthePump

This chapter explains the operational parameters of the binary pump.

5 Optimizing Performance

This chapter gives information on how to optimize the performance of the

Binary Pump under special operational conditions.

6 Troubleshooting and Diagnostics

Overview of the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 1260 Infinity Binary Pump User Manual

In This Guide...

8 Test Functions and Calibration

This chapter explains all test functions that are available for the binary

pump.

9 Diagnostic Signals

This chapter explains all diagnostic signals of the binary pump.

10 Maintenance

This chapter describes the maintenance of the module.

11 Parts and Materials for Maintenance

This chapter lists all parts and tools that are required for maintenance.

12 Identifying Cables

This chapter provides information on cables used with the Agilent 1200

Infinity Series modules.

13 Hardware Information

This chapter provides detailed technical information about your binary

pump.

14 Appendix

This appendix provides general safety and environmental information.

1260 Infinity Binary Pump User Manual 5

Contents

1 Introduction to the Binary Pump 9

Instrument and Operation 10

Overview of the Hydraulic Path 13

Leak and Waste Handling 18

2 Site Requirements and Specifications 21

Site Requirements 22

Physical Specifications 25

Performance Specifications 26

3 Installing the Pump 29

Unpacking the Binary Pump 30

Optimizing the Stack Configuration 33

Installation Information on Leak and Waste Handling 41

Installing the Binary Pump 45

Flow Connections with Solvent Selection Valve 48

Flow Connections without Solvent Selection Valve 51

Priming the System 54

4UsingthePump 59

Leak and Waste Handling 60

Hints for Successful Use of the Binary Pump 61

Setting up the Pump with the G4208A Instant Pilot 62

Setting up the Agilent 1260 Infinity Binary Pump G1312B with the Instrument

Control Interface 63

Solvent Information 69

Algae Growth in HPLC Systems 74

Prevent Blocking of Solvent Filters 76

6 1260 Infinity Binary Pump User Manual

Contents

5 Optimizing Performance 79

When to Use a Vacuum Degasser 80

When to Use the Active Seal Wash Option 81

When to Use Alternative Seals 82

When to Use the Low Volume Mixer 83

When to Remove Damper and Mixer 84

How to Optimize the Compressibility Compensation Setting 87

6 Troubleshooting and Diagnostics 91

Overview of the Module’s Indicators and Test Functions 92

Status Indicators 94

User Interfaces 96

Agilent Lab Advisor Software 97

7 Error Information 99

What Are Error Messages 101

General Error Messages 102

Module Error Messages 109

8 Test Functions and Calibration 125

(System) Pressure Test 126

Valve Test 131

Binary Pump Solvent Compressibility Calibration 133

Pump Elasticity Calibration 135

Leak Rate Test 137

9 Diagnostic Signals 143

Analog Pressure Output 144

Diagnostic Signals in Chromatographic Data Systems 145

1260 Infinity Binary Pump User Manual 7

Contents

10 Maintenance 147

Introduction to Maintenance and Repair 148

Warnings and Cautions 149

Cleaning the Module 151

Overview of Maintenance and Simple Repairs 152

Maintenance Procedures 153

Exchanging the Purge Valve Frit or the Purge Valve 154

Removing the Pump Head Assembly 157

Maintenance of a Pump Head without Seal Wash 159

Maintenance of a Pump Head with Seal Wash 163

Reinstalling the Pump Head Assembly 167

Seal Wear-in Procedure 169

Exchanging the Active Inlet Valve (AIV) or its Cartridge 170

Exchanging the Outlet Valve 173

Installation of the Solvent Selection Valve Upgrade Kit 175

Exchanging the Solvent Selection Valve 177

Exchanging the Optional Interface Board 180

Replacing Module Firmware 181

11 Parts and Materials for Maintenance 183

Hydraulic Path with Solvent Selection Valve 184

Hydraulic Path without Solvent Selection Valve 186

Pump Head Assembly Without Seal Wash 188

Pump Head Assembly with Seal Wash Option 190

Outlet Valve 192

Purge Valve Assembly 193

Active Inlet Valve Assembly 194

HPLC Starter Kit G4201-68707 195

HPLC Starter Kit G4202-68707 195

HPLC System Tool Kit 196

Bottle Head Assembly 197

Solvent Cabinet 198

8 1260 Infinity Binary Pump User Manual

Contents

12 Identifying Cables 201

Overview 202

Analog cables 204

Remote Cables 206

BCD Cables 209

CAN/LAN Cables 211

External Contact Cables 212

RS-232 Cable Kit 213

Agilent 1200 Module to Printer 214

13 Hardware Information 215

Firmware Description 216

Electrical Connections 219

Interfaces 221

Setting the 8-bit Configuration Switch (without On-board) LAN 228

Optional Interface Boards 232

The Solvent Selection Valve (SSV) 236

Early Maintenance Feedback 237

Instrument Layout 238

14 Appendix 239

General Safety Information 240

The Waste Electrical and Electronic Equipment Directive 243

Lithium Batteries Information 244

Radio Interference 245

Sound Emission 246

Agilent Technologies on the Internet 247

1260 Infinity Binary Pump User Manual

Agilent Technologies

Introduction to the Binary Pump

Instrument and Operation 10

Introduction to the Pump 10

Principle of Operation 11

Overview of the Hydraulic Path 13

Leak and Waste Handling 18

This chapter gives an introduction to the module and an instrument overview.

10 1260 Infinity Binary Pump User Manual

1Introduction to the Binary Pump

Instrument and Operation

Introduction to the Pump

The binary pump comprises two identical pumps integrated into one

housing. Binary gradients are created by high- pressure mixing. An

optional degasser is available for applications that require best flow

stability, especially at low flow rates, for maximum detector sensitivity.

Pulse damper and mixer can be bypassed for low flowrate applications or

whenever a minimal transient volume is desirable. Typical applications are

high throughput methods with fast gradients on high resolution 2.1 mm

columns. The pump is capable of delivering flow in the range of 0.1 –

5 mL/min against up to 600 bar. A solvent selection valve (optional)

allows to form binary mixtures (isocratic or gradient) from one of two

solvents per channel. Active seal wash (optional) is available for use with

concentrated buffer solutions.

Figure 1 Overview of the binary pump

Purge valve

Active inlet valve

Mixer

Outlet valve

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