Agilent Technologies InfinityLab LC Series Manuale utente

Agilent InfinityLab LC Series

1260 Infinity II Binary Pump

User Manual

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual

Notices

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Document No: SD-29000214 Rev. C

Edition: 10/2021

No part of this manual may be repro-

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InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 3

In This Guide...

This manual covers the Agilent InfinityLab LC Series 1260 Infinity II Binary Pump

(G7112B).

1Introduction

This chapter gives an introduction to the module and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information about site requirements and specifications for

the binary pump.

3UsingthePump

This chapter explains the operational parameters of the Binary Pump.

4 Optimizing Performance

This chapter gives information on how to optimize the performance of the Binary

Pump under special operational conditions.

5Troubleshootingand Diagnostics

Overview of the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides information

on probable causes and suggested actions how to recover from error conditions.

7 Test Functions and Calibration

This chapter explains all test functions that are available for the binary pump.

8 Maintenance

This chapter describes the maintenance of the module.

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 4

9 Parts and Materials for Maintenance

This chapter lists all parts and tools that are required for maintenance and simple

repairs.

10 Identifying Cables

This chapter provides information on cables used with the Agilent InfinityLab LC

Series modules.

11 Hardware Information

This chapter provides detailed technical information about your binary pump.

12 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

13 Appendix

This chapter provides addition information on safety, legal and web.

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 5

Contents

1Introduction10

Instrument and Operation 11

Overview of the Hydraulic Path 15

Leak and Waste Handling 20

2 Site Requirements and Specifications 25

Site Requirements 26

Physical Specifications 29

Performance Specifications 30

3UsingthePump32

Magnets 33

Turn on/off 34

Status Indicators 36

Best Practices 37

Leak and Waste Handling 39

Hints for Successful Use of the Binary Pump 40

Setting up the Pump with the G4208A Instant Pilot 41

Setting up the Pump with the Instrument Control Interface 42

Solvent Information 47

Algae Growth in HPLC Systems 54

Prevent Blocking of Solvent Filters 55

Normal Phase Applications 57

4 Optimizing Performance 59

When to Use a Vacuum Degasser 60

When to Use the Active Seal Wash Option 61

When to Use the Low Volume Mixer 62

When to Remove Damper and Mixer 63

How to Optimize the Compressibility Compensation Setting 65

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 6

5 Troubleshooting and Diagnostics 68

Overview of the Module’s Indicators and Test Functions 69

User Interfaces 71

Agilent Lab Advisor Software 72

6 Error Information 73

What Are Error Messages 74

General Error Messages 75

Module Error Messages 81

7 Test Functions and Calibration 92

(System) Pressure Test 93

Valve Test 98

Binary Pump Solvent Compressibility Calibration 100

Pump Elasticity Calibration 102

Pump Leak Rate Test 104

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 7

8 Maintenance 108

Introduction to Maintenance 109

Cautions and Warnings 110

Cleaning the Module 112

Overview of Maintenance and Simple Repairs 113

Maintenance Procedures 114

Remove and Install Doors 115

Exchange the Purge Valve Frit or the Purge Valve 117

Replace the O-Ring on the Purge Valve 120

Remove the Pump Head Assembly 122

Maintenance of a Pump Head without Seal Wash 124

Maintenance of a Pump Head with Seal Wash 127

Reinstall the Pump Head Assembly 131

Seal Wear-in Procedure 133

Exchange the Active Inlet Valve (AIV) or its Cartridge 134

Exchange the Seal Wash Cartridge 137

Replace Leak Handling System Parts 139

Exchange the Outlet Valve 141

Installation of the Solvent Selection Valve Upgrade Kit 143

Exchange the Solvent Selection Valve 145

Replacing Module Firmware 148

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 8

9 Parts and Materials for Maintenance 149

Hydraulic Path with Solvent Selection Valve 150

Hydraulic Path without Solvent Selection Valve 152

Pump Head Assembly Without Seal Wash 154

Pump Head Assembly with Seal Wash Option 156

Outlet Valve 158

Purge Valve Assembly 159

Active Inlet Valve Assembly 160

HPLC System Tool Kit 161

Active Seal Wash Option 162

Solvent Cabinet 163

Bottle Head Assembly 164

Accessory Kit 165

Cover Parts 166

10 Identifying Cables 167

Cable Overview 168

Analog Cables 170

Remote Cables 172

CAN/LAN Cables 176

RS-232 Cable Kit 177

Agilent 1200 Module to Printer 178

11 Hardware Information 179

Firmware Description 180

Electrical Connections 183

Interfaces 185

Setting the 6-bit Configuration Switch 193

Early Maintenance Feedback 197

Instrument Layout 198

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 9

12 LAN Configuration 199

What You Have to Do First 200

TCP/IP parameter configuration 201

Configuration Switches 202

Initialization Mode Selection 203

Dynamic Host Configuration Protocol (DHCP) 205

Manual Configuration 208

13 Appendix 212

General Safety Information 213

Waste Electrical and Electronic Equipment (WEEE) Directive 219

Radio Interference 220

Sound Emission 221

Agilent Technologies on the Internet 222

InfinityLab LC Series 1260 Infinity II Binary Pump User Manual 10

1Introduction

Instrument and Operation 11

Introduction to the Pump 11

Principle of Operation 12

Product Description 14

Features 14

Overview of the Hydraulic Path 15

Leak and Waste Handling 20

Leak Sensor 23

Waste Concept 24

This chapter gives an introduction to the module and an instrument overview.

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