Agilent Technologies G7050A Istruzioni per il montaggio

G7050A - Reference Compound

Introduction Valve for the Agilent 7010

Triple Quadrupole

Installation and Setup Guide

2 G7050A - Reference Compound Introduction Valve

Contents

Parts Supplied 3

Separate the MS from the GC 4

Separate the MS and the 8890 or 7890 GC 4

Separate the MS and the 9000 GC 5

Remove the MS Covers 7

Attach the Voltage Divider Board 9

Install the Reference Compound Valve 11

Install the MS Wiring Harness 13

Install the MS Covers 16

Install the Front Cover 16

Install the MS Top Cover 17

Remove the GC Covers 18

Remove the 7890/8890 GC Covers 18

Install the 7890/8890 GC Wiring Harness 21

Install the 9000 GC Control Wiring 23

Remove the 9000 GC cover 23

Install the GC wiring harness in the 9000 GC 24

Install the 9000 GC covers 24

Attach the MS and GC 25

Attach the MS to the 8890 or 7890 GC 25

Attach the MS and the 9000 GC 26

Edit the GC Method 29

Configuring the reference valve 29

Add a Timed Event to the method 30

Verify the correct column is installed 31

Edit MS method parameters 32

Add a PFTBA Reference Compound to an MRM method 32

Add a valve Monitor to the method 33

Maintenance 34

To Refill the Reference Compound Valve Vial 34

Troubleshooting 35

Performance 35

Hardware 36

Warranty 37

G7050A - Reference Compound Introduction Valve 3

Parts Supplied

The G7050A - Reference Compound Introduction Valve for the Agilent 7010

Triple Quadrupole accessory kit includes the following parts:

Table 1 Parts supplied with the Reference Compound Introduction Valve kit

Item Description Qty Part Number

1 MS Wiring Harness 1 G7006-81001

2 8890/9000 GC Wiring Harness 1 G7006-81002

3 Reference Compound Valve 1 G7006-60207

4 Torx-T20 M4 x 0.7 12 MM Lg w/crest washer for mounting PCA voltage divider 2 0515-0382

5 Aluminum mounting block for PCA voltage divider 1 G7006-00101

6 PCA Voltage Divider Board 1 G7006-61001

7 O-ring 6.07 1.75 FKM 75A BRN 3 0905-1014

8 Dual Adapter Assembly for mounting valves to the Analyzer Manifold 1 G7006-60210

9 Torx-T20 M 4 x 0.7 45MM Lg w/crest washer for mounting Reference Valve 2 0515-0670

10 GCMS Tuning Standard - PFTBA 0.5 mL (will be shipped separately from the kit) 1 05971-60571

Figure 1. Parts supplied with the Reference Compound Introduction Valve kit

123

566

8 9

4 G7050A - Reference Compound Introduction Valve

Separate the MS from the GC

If using an 8890 or 7890 GC see “Separate the MS and the 8890 or 7890 GC” below.

If using a 9000 GC see “Separate the MS and the 9000 GC” on page 5.

Separate the MS and the 8890 or 7890 GC

Materials needed

•T-20 Torx drivers

•Ferrule, blank (5181-3308)

•Interface column nut (05988-20066)

•Wrench, open-end, 1/4-inch × 5/16-inch (8710-0510)

•Gloves, clean, lint-free (Large 8650-0030) (Small 8650-0029)

Procedure

1Vent the MS. Refer to the Agilent 7000/7010 Series TQ GC/MS Operating Manual.

2Turn off the GC and MS and remove their power cables from the building supply mains.

Remove the capillary column from the GC/MS interface.

3Place a column nut with a blank ferrule on the end of the interface. This will help keep

contamination out of the MS. The foreline pump may be located on the floor or on the lab

table next to or behind the MS,. Move it as needed to provide slack in the tubing and cables.

4Move the MS away from the GC until you have access to the GC/MS interface cable. See

Figure 2 on page 5.

WARNING Ensure the GC/MS interface and the analyzer zones are cool (below 100 °C) before you

vent the MS. A temperature of 100 °C is hot enough to burn skin; always wear cloth gloves

when handling analyzer parts.

WARNING Ensure the GC/MS interface and GC oven have cooled before you remove the column.

WARNING If you are using hydrogen as a carrier gas or for a system with JetClean installed, the

carrier gas flow and JetClean hydrogen supply shutoff valves must be closed before

turning off the MS power. If the foreline pump is off, hydrogen will accumulate in the MS

and an explosion may occur. Before operating the MS with hydrogen carrier gas read the

hydrogen safety information. (See Hydrogen Safety on page 16.)

CAUTION Ensure the GC oven and the GC/MS interface are cool before turning off carrier gas flow.

G7050A - Reference Compound Introduction Valve 5

5Disconnect the GC/MS interface cable. If the MS needs to be moved a significant distance

from the GC, also disconnect the APG cable and the LVDS cable if used.

Separate the MS and the 9000 GC

Materials needed

•Screwdriver, T-20 Torx

•Ferrule, blank (5181-3308)

•MS transfer line plug (G4590-60250)

•Gloves, white, nylon, clean, lint-free (Large 8650-0030) (Small 8650-0029)

Figure 2. Separating/connecting the MS and 8890/7890 GC

WARNING Ensure the GC/MS interface and the analyzer zones are cool (below 100 °C) before you

vent the MS and remove the 9000 GC/MS Tail. A temperature of 100 °C is hot enough to

burn skin; always wear cloth gloves when handling analyzer parts.

WARNING If you are using hydrogen as a carrier gas or for a system with JetClean installed, the

carrier gas flow and JetClean hydrogen supply shutoff valves must be closed before

turning off the MS power. If the foreline pump is off, hydrogen will accumulate in the MS

and an explosion may occur. Before operating the MS with hydrogen carrier gas read the

hydrogen safety information.

CAUTION Ensure the GC oven and the GC/MS interface are cool before turning off carrier gas flow.

6 G7050A - Reference Compound Introduction Valve

Procedure

1Vent the MS. Refer to the Agilent 7000/7010 Series TQ GC/MS Operating Manual.

2Remove the 9000 GC/MS Tail. Refer to the Agilent 7000/7010 Series TQ GC/MS

Operating Manual.

3Verify that the GC and MS are turned off and that their power cables are unplugged from

the building supply mains.

4Using a T-20 Torx screwdriver, loosen the lock plate by turning the lock plate screw

clockwise.

5The foreline pump may be located on the floor, on the lab bench next to or behind the MS.

Move it as needed to provide slack in the tubing and cables.

6Slide the MS backwards, and then away from the GC until you have access to the GC/MS

cables. (See Figure 3 on page 6.)

7Disconnect the GC/MS interface cables. Disconnecting the cable with the GC on can cause

a fault condition. If the MS needs to be moved a significant distance from the GC, also

disconnect the APG cable and the LVDS cable if used.

8Install an MS transfer line plug and blank ferrule on the end of the GC/MS interface. This

will help keep contamination out of the MS.

Figure 3. Separating/connecting the MS and 9000 GC

G7050A - Reference Compound Introduction Valve 7

Remove the MS Covers

Materials needed

•Screwdriver, Torx T-20 (8710-1615)

Procedure

For detailed cover removal instructions, refer to the Maintaining the Mainframe section in the

Agilent 7000/7010 Series Triple Quadrupole Troubleshooting and Maintenance Manual.

1Remove the analyzer window cover. See Figure 4 below.

Figure 4. MS covers

Analyzer window cover Top cover

Left side panel

Front bottom cover

8 G7050A - Reference Compound Introduction Valve

2Remove the front bottom cover by gasping the cover on both sides and gently pulling the

cover forward so you can remove the LED cable.

3Use a T-20 screwdriver to remove the seven screws securing the MS top cover.

Figure 5. Removing the LED cable

Figure 6. Removing MS top cover. Cutout shown is for Instruments with CI or JetClean flow modules

G7050A - Reference Compound Introduction Valve 9

Attach the Voltage Divider Board

Materials needed

•Voltage divider board (Figure 1 item 6)

•Aluminum mounting block for voltage divider board (Figure 1 item 5)

•Two screws (Figure 1 item 4)

Procedure

1Use a T-20 screwdriver to remove the one or two screws, depending on MS model,

attaching the sheet metal baffle to the e-module.

2If your MS model includes a LED, remove the LED cable from the plastic holder.

Figure 7. Remove screws from the metal baffle

Figure 8. Remove cable from the plastic holder

10 G7050A - Reference Compound Introduction Valve

3Use a screwdriver to pry out the top right corner of the sheet metal baffle and remove it

from the MS.

4Align the screw holes in the PCA voltage divider board (Figure 1 item 6) and Aluminum

mounting block (Figure 1 item 5), with the tapped screw holes in the front electronics

module frame. Use a T20 driver to attach this PCA board and mounting block using two

screws (Figure 1 item 4) threaded into the frame (arrows).

PCA

Figure 9. Remove the baffle

Figure 10. Attaching the PCA voltage divider board and Aluminum mounting block with two screws

Electronics module frame

PCA board

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