Agilent Technologies 5100 ICP-OES Istruzioni operative

Agilent 5100 and 5110

ICP-OES

Site Preparation Guide

2 Agilent 5100 and 5110 ICP-OES Site Preparation Guide

Notices

2014, 2016, 2017, 2019

No part of this manual may be

reproduced in any form or by any

means (including electronic storage

and retrieval or translation into a

foreign language) without prior

agreement and written consent from

Agilent Technologies, Inc. as governed

by United States and international

Manual Part Number

G8010-90001

Edition

Fifth edition, February 2019

Agilent Technologies, Australia (M)

Pty Ltd

679 Springvale Road

Mulgrave, Victoria, 3170

Australia

www.agilent.com

Warranty

The material contained in this

document is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further, to

the maximum extent permitted by

applicable law, Agilent disclaims all

warranties, either express or implied,

with regard to this manual and any

information contained herein,

including but not limited to the

implied warranties of merchantability

and fitness for a particular purpose.

Agilent shall not be liable for errors

or for incidental or consequential

damages in connection with the

furnishing, use, or performance of

this document or of any information

contained herein. Should Agilent and

the user have a separate written

agreement with warranty terms

covering the material in this

document that conflict with these

terms, the warranty terms in the

separate agreement shall control.

Technology Licenses

The hardware and/or software

described in this document are

furnished under a license and may be

used or copied only in accordance

with the terms of such license.

Restricted Rights Legend

If software is for use in the

performance of a U.S. Government

prime contract or subcontract,

Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June

1995), or as a “commercial item” as

defined in FAR 2.101(a) or as

“Restricted computer software” as

defined in FAR 52.227-19 (June 1987)

or any equivalent agency regulation or

contract clause. Use, duplication or

disclosure of Software is subject to

Agilent Technologies’ standard

commercial license terms, and non-

DOD Departments and Agencies of the

U.S. Government will receive no

greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will

receive no greater than Limited Rights

as defined in FAR 52.227-14 (June

1987) or DFAR 252.227-7015 (b)(2)

(November 1995), as applicable in any

technical data.

Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed or

adhered to, could result in personal

injury or death. Do not proceed

beyond a WARNING notice until the

indicated conditions are fully

understood and met.

WARNING

CAUTION

Request for Installation

Agilent 5100 and 5110 ICP-OES Site Preparation Guide 3

Request for Installation

All preparations have been completed. Please arrange for the

installation to be completed as soon as possible. I understand that if

the installation site is not prepared in accordance with the enclosed

instructions, additional installation charges may apply.

Company name:

Company address:

Name:

Position:

Telephone:

Preferred installation date:

Signed:

Date:

Site Preparation Checklist

4 Agilent 5100 and 5110 ICP-OES Site Preparation Guide

Site Preparation Checklist

Your site must meet all requirements before you request installation.

Complete each requirement listed in the table. After completing each

requirement, place a check in the appropriate check box. Ensure you

compare the boxes with the shipping list supplied with the boxes.

Requirements



Principal installation area is in compliance with all relevant safety regulations.



Laboratory temperature is maintained between 15-30°C (59-86°F)



Laboratory is free of excessive particulate matter.



Cooling air system is set up (if required).



Workbench requirements are met.



Sufficient bench space is available for all components.



Bench can support system weight.



Personal computer with Microsoft Windows 7 Professional 64-bit SP1 or Microsoft Windows 10

Professional installed and printer is set up, if purchased separately.



Exhaust system is suitable and installed.



Specified electrical supply and power outlets are installed.



Gas supply (at specified purity), regulator, and gas lines are installed for argon and any allowed optional

gases.



Water cooling/circulation system and power connections are set up, if system is not purchased from

Agilent.



Waste container appropriate for the chemical waste is prepared.



Accessories Purchased

SPS 4 Autosampler



SPS 3 Sample Preparation System



Advanced valve system (AVS) 4, 6, or 7 Switching Valve



SVS 2+ Productivity Package



VGA Vapor Generation Accessory



5 Channel Peristaltic Pump



Air Inlet Duct Filter



External Inlet Duct Adapter



Multimode Sample Introduction System (MSIS)



Argon Saturator Accessory (ASA)



IsoMist™ Programmable Temperature Spray Chamber



Contents

Agilent 5100 and 5110 ICP-OES Site Preparation Guide 5

Contents

Request for Installation 3

Site Preparation Checklist 4

1. Safety Practices and Hazards 7

Heat, Vapors and Fumes 7

Compressed Gas Hazards 7

Electrical Hazards 8

Other Precautions 8

2. Introduction 9

Installation Guidelines 9

3. Laboratory Environment 11

Environmental Conditions 11

Installation category 11

Pollution level 11

Temperature Control 12

Cleanliness 12

Instrument Cooling Air Supply 12

Workbench 13

Location 14

PC Requirements 17

4. Instrument Shipping Information 19

Weights and Dimensions 19

Safety Practices and Hazards

6 Agilent 5100 and 5110 ICP-OES Site Preparation Guide

Seismic Requirements 20

5. Laboratory Facilities 23

Exhaust System 23

Electrical Power Supplies 25

Electrical Requirements 26

Single phase requirement 26

Power plugs and cords 27

Gas Supplies 27

Water Chiller System 30

Location 31

Waste Fluid Container 32

Guidelines for Software Installation 32

6. Accessories and Options 34

Vapor Generation Accessory (VGA) Recommended Gases 34

Important Customer Web Links 35

Appendix A: Power Cords 36

Safety Practices and Hazards

Agilent 5100 and 5110 ICP-OES Site Preparation Guide 7

1. Safety Practices and Hazards

Heat, Vapors and Fumes

Heat, ozone, vapors and fumes generated by the plasma can be

hazardous, and must be extracted from the instrument by means of

an exhaust system. Ensure that an exhaust system of the appropriate

type is fitted (see Page 23). The system must be vented to the outside

air in accordance with local regulations and never within the

building. Regularly check the exhaust system by smoke test to ensure

that the exhaust system is functioning correctly. The exhaust fan

must always be switched on before igniting the plasma.

Compressed Gas Hazards

All compressed gases (other than air) can create a hazard if they leak

into the atmosphere. Even small leaks in gas supply systems can be

dangerous. Any leak (except that of air or oxygen) can result in an

oxygen-deficient atmosphere, which can cause asphyxiation. The

area in which cylinders are stored and the area surrounding the

instrument must be adequately ventilated to prevent such gas

accumulations.

Gas cylinders must be installed, stored and handled strictly in

accordance with local safety codes and regulations. Cylinders must

be used and stored only in a vertical position and secured to an

immovable structure or a properly constructed cylinder stand. Move

cylinders only by securing them to a properly constructed trolley.

Use only approved regulator and hose connectors (refer to the gas

supplier’s instructions).

Safety Practices and Hazards

8 Agilent 5100 and 5110 ICP-OES Site Preparation Guide

Use only ‘instrument grade’ gases with your spectrometer.

If using cryogenic gases (for example, liquid argon), prevent severe

burns by wearing suitable protective clothing and gloves.

Electrical Hazards

Connecting the Agilent ICP-OES to a power source that is not

equipped with a protective earth contact creates a shock hazard for

the operator and can damage the instrument. Likewise, interrupting

the protective conductor inside or outside the Agilent ICP-OES or

defeating the power cord ground creates a shock hazard for the

operator and can damage the instrument.

Other Precautions

Air flow to the cooling fans of the spectrometer and accessories must

be unobstructed. Do not block the ventilation grills on the

spectrometer and accessories. Consult the manuals supplied with

your PC, monitor, printer and water-cooling system for their specific

ventilation requirements.

The spectrometer weighs approximately 106 kg (234 lb). To avoid

injury to personnel or damage to the instrument or property, always

use a forklift or other suitable mechanical lifting device to move the

instrument.



After all safety regulations have been met, check the checklist box: Principal installation

area is in compliance with all relevant safety regulations.

Introduction

Agilent 5100 and 5110 ICP-OES Site Preparation Guide 9

2. Introduction

This publication contains the information required to successfully

prepare a site for an Agilent ICP-OES system installation.

On completion of the site preparation, fill in the checklist on Page 4,

(striking out those entries not applicable), and send this checklist to

your local Agilent agent or Agilent sales and service office. As soon

as it is received, Agilent or its agent will contact you to arrange a

convenient time for installation.

If you have difficulty in preparing for the installation, and for details

of operator training courses, please contact your Agilent sales or

field service representative.

Installation Guidelines

Allow a minimum of one day for the installation of the Agilent

ICP-OES system by an Agilent field service engineer.

The installation will include the following:

Spectrometer installation

Water chiller connection

Instrument software installation and registration

Accessory installation

Spectrometer installation performance tests

Basic customer training

Maintenance overview

Introduction

10 Agilent 5100 and 5110 ICP-OES Site Preparation Guide

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