Agilent Technologies Infinity Binary Pump VL 1290 Manuale utente

Agilent Technologies

Agilent 1290 Infinity

Binary Pump VL

User Manual

Agilent 1290 Infinity Binary Pump User Manual

Notices

2010-2012

No part of this manual may be reproduced

in any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G4220-90005 Rev. C

Edition

08/2012

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

This product may be used as a com-

ponent of an in vitro diagnostic sys-

tem if the system is registered with

the appropriate authorities and com-

plies with the relevant regulations.

Otherwise, it is intended only for gen-

eral laboratory use.

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation

or contract clause. Use, duplication or dis-

closure of Software is subject to Agilent

Technologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully under-

stood and met.

Agilent 1290 Infinity Binary Pump User Manual 3

In This Guide…

This manual covers the Agilent 1290 Infinity Binary Pump (G4220B).

1 Introduction

This chapter gives an introduction to the pump, instrument overview and

internal connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3 Installing the Module

This chapter gives information about the preferred stack setup for your system

and the installation of your Agilent 1290 Infinity Binary Pump.

4UsingthePump

This chapter explains the operational parameters of the Agilent 1290 Infinity

Binary Pump.

5 How to Optimize the Performance of Your Module

This chapter gives hints on how to optimize the performance or use additional

devices.

6 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

7 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

4 Agilent 1290 Infinity Binary Pump User Manual

In This Guide…

8 Test Functions and Calibrations

This chapter describes the tests for the module.

9 Maintenance

This chapter describes the maintenance of the Agilent 1290 Infinity Binary

Pump.

10 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

11 Identifying Cables

This chapter summarizes information on all cables.

12 Hardware Information

This chapter describes the pump in more detail on hardware and electronics.

13 LAN Configuration

This chapter provides information on connecting the detector to the Agilent

ChemStation PC.

14 Appendix

This chapter provides addition information on safety, legal and web.

Agilent 1290 Infinity Binary Pump User Manual 5

Contents

1 Introduction 9

Features 10

Overview of the Binary Pump 11

Pump Principle 12

2 Site Requirements and Specifications 15

Site Requirements 16

Physical Specifications 19

Specifications 20

3 Installing the Module 23

Unpacking the Module 24

Optimizing the Stack Configuration 26

Removing the Transport Foam 31

Installing the Pump 32

Flow connections to the pump 35

Installation of seal wash option 39

4UsingthePump 41

Preparing the Binary Pump 42

Algae Growth in HPLC Systems 43

Setting up the Pump with the Instrument Control Interface 44

Priming the Pump 54

Solvent Information 56

5 How to Optimize the Performance of Your Module 61

Delay Volume and Extra-Column Volume 62

How to Configure the Optimum Delay Volume 63

How to Achieve Higher Resolution 65

Using Solvent Calibration Tables 68

6 Agilent 1290 Infinity Binary Pump User Manual

Contents

6 Troubleshooting and Diagnostics 69

Overview of the Module’s Indicators and Test Functions 70

Status indicators 71

Available Tests vs User Interfaces 73

Agilent Lab Advisor Software 74

7 Error Information 75

What Are Error Messages 77

General Error Messages 78

Pump Error Messages 85

8 Test Functions and Calibrations 101

Introduction 102

System Pressure Test 103

Pump Head Leak Test 105

9 Maintenance 109

Introduction to Maintenance 110

Warnings and Cautions 112

Overview of Maintenance 113

Cleaning the Module 114

Installing Fittings and Capillaries 115

Replacing the Shutoff Valve Panel 116

Replacing the Pressure Sensor 118

Replacing the Inlet valve 120

Replacing the Outlet valve 122

Replacing the Solvent Selection Valve (SSV) 125

Changing configuration or replacing the Jet Weaver 127

Replacing the Seal Wash Pump 130

Releasing a Stuck Inlet Valve 131

Replacing the Pump Heads 134

Disassembling the Pump Head 139

Disassembling the Primary Pump Head 140

Disassembling the Secondary Pump Head 143

Assembling the Pump Head 146

Replacing the Purge Valve Head 154

Replacing Parts of the High Pressure Filter Assembly 157

Agilent 1290 Infinity Binary Pump User Manual 7

Contents

Installing the Valve Rail Kit 159

Replacing the Main Power Fuses 160

Replacing Module Firmware 162

Preparing the Pump Module for Transport 163

10 Parts and Materials for Maintenance 167

Overview of Maintenance Parts 168

Capillaries 169

Solvent Cabinet Kit 170

Seal Wash Option 171

Pump Head Assembly Parts 172

Primary Pump Head Parts 174

Secondary Pump Head Parts 178

Purge Valve 182

Cover Parts 183

Leak Parts 184

Fuses 184

Accessory Kit 185

Others 186

11 Identifying Cables 189

Cable Overview 190

Analog cables 192

Remote Cables 194

BCD Cables 197

CAN/LAN Cable 199

RS-232 Cable Kit 200

Agilent 1200 Module to Printer 201

12 Hardware Information 203

Firmware Description 204

Electrical Connections 207

Interfaces 209

Setting the 8-bit Configuration Switch 216

Instrument Layout 220

Early Maintenance Feedback 221

8 Agilent 1290 Infinity Binary Pump User Manual

Contents

13 LAN Configuration 223

What You Have to Do First 224

TCP/IP parameter configuration 226

Configuration Switch 227

Initialization mode selection 228

Dynamic Host Configuration Protocol (DHCP) 232

Link configuration selection 236

Automatic configuration with Bootp 237

Manual Configuration 247

PC and User Interface Software Setup Setup 253

14 Appendix 255

General Safety Information 256

The Waste Electrical and Electronic Equipment (WEEE) Directive

(2002-96-EC) 259

Radio Interference 260

Sound Emission 261

Agilent Technologies on Internet 262

Agilent 1290 Infinity Binary Pump User Manual

Agilent Technologies

Introduction

Features 10

Overview of the Binary Pump 11

Pump Principle 12

This chapter gives an introduction to the pump, instrument overview and

internal connectors.

10 Agilent 1290 Infinity Binary Pump User Manual

1Introduction

Features

The Binary pump is designed for highest performance, GLP compliance and

easy maintenance. It includes the following features:

•Seal wash for continued high lifetime of pump seals using high buffer

concentrations.

•Solvent selection valve for method flexibility.

•Jet Weaver for optimum mixing performance with a minimum of delay

volume.

•Automatic purge function for ease of use and unattended preparation of the

system.

•Auto tuning of the delivery cycle for compensation of elasticity and dead

volume effects.

•Solvent selection for optimum density correction.

•Fast defill function to increase robustness of the pump.

•Two pistons in series design for increased reliability.

•Smooth motion control to prevent shock movements.

For specifications, see Table 2 on page 20.

NOTE

This Binary pump has been introduced together with the Agilent 1290 Infinity Liquid

Chromatograph.

Indice

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