Agilent Technologies 7820A Istruzioni per il montaggio
Agilent Technologies
Agilent 7820A
Gas Chromatograph
Advanced User Guide
Notices
Agilent Technologies, Inc. 2016
No part of this manual may be reproduced
in any form or by any means (including
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tion into a foreign language) without prior
agreement and written consent from
Agilent Technologies, Inc. as governed by
United States and international copyright
laws.
Manual Part Number
G4350-90020
Edition
Fifth edition, August 2016
Fourth edition, September 2015
Third edition, June 2011
Second edition, January 2010
First edition, March 2009
Printed in China
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Shanghai 200131 P.R.China
Technology Licenses
The hardware and/or software described in
this document are furnished under a
license and may be used or copied only in
accordance with the terms of such license.
Restricted Rights
If software is for use in the performance of
a U.S. Government prime contract or sub-
contract, Software is delivered and
licensed as “Commercial computer soft-
ware” as defined in DFAR 252.227-7014
(June 1995), or as a “commercial item” as
defined in FAR 2.101(a) or as “Restricted
computer software” as defined in FAR
52.227-19 (June 1987) or any equivalent
agency regulation or contract clause. Use,
duplication or disclosure of Software is
subject to Agilent Technologies’ standard
commercial license terms, and non-DOD
Departments and Agencies of the U.S. Gov-
ernment will receive no greater than
Restricted Rights as defined in FAR
52.227-19(c)(1-2) (June 1987). U.S. Govern-
ment users will receive no greater than
Limited Rights as defined in FAR 52.227-14
(June 1987) or DFAR 252.227-7015 (b)(2)
(November 1995), as applicable in any
technical data.
Safety Notices
CAUTION
A CAUTION notice denotes a hazard. It
calls attention to an operating
procedure, practice, or the like that, if
not correctly performed or adhered to,
could result in damage to the product
or loss of important data. Do not
proceed beyond a CAUTION notice
until the indicated conditions are fully
understood and met.
WARNING
A WARNING notice denotes a hazard.
It calls attention to an operating
procedure, practice, or the like that, if
not correctly performed or adhered to,
could result in personal injury or
death. Do not proceed beyond a
WARNING notice until the indicated
conditions are fully understood and
met.
Firmware Version
This manual is written for 7820A GCs using
firmware version A.01.18.
Advanced User Guide 3
Contents
1 Software Keypad
Using the Software Keypad 10
2 Programming
Run Time Programming 12
Using run time events 12
Programming run time events 13
The run table 13
Adding events to the run table 13
Editing events in the run table 14
Deleting run time events 14
Clock Time Programming 15
Using clock time events 15
Programming clock time events 15
Adding events to the clock table 15
Editing clock time events 16
Deleting clock time events 16
Post Run Programming 17
To enable a post run program 17
To disable a post run program 17
3 Inlets
Using Hydrogen 20
Inlet Overview 21
Carrier Gas Flow Rates 22
About Gas Saver 23
To use gas saver 24
Pre Run and Prep Run 25
The [Prep Run] key 25
Auto Prep Run 26
About the Split/Splitless Inlet 27
Septum tightening (S/SL) 27
Standard S/SL inlet 28
Split/Splitless inlet split mode overview 28
Split/Splitless inlet splitless mode overview 29
The S/SL inlet pulsed split and splitless modes 30
Split/Splitless inlet split mode minimum operating pressures 31
4 Advanced User Guide
Selecting the correct S/SL inlet liner 32
Vapor Volume Calculator 34
Setting parameters for the S/SL split mode 34
Selecting parameters for the S/SL splitless mode 36
Setting parameters for the S/SL splitless mode 36
Setting parameters for the S/SL pulsed modes 38
About the Purged Packed Column Inlet 39
Setting parameters 40
About the Packed Column Inlet 41
Adjusting parameters 42
About the Cool On-Column Inlet 43
Setup modes of the COC inlet 44
Retention gaps 44
COC inlet temperature control 44
Setting COC inlet flows/pressures 45
Setting COC inlet parameters 46
4 Columns and Oven
About the Oven 48
Oven safety 48
Configuring the Oven 49
About Oven Temperature Programming 50
Programming setpoints 50
Oven ramp rates 51
Setting the oven parameters for constant temperature 51
Setting the oven parameters for ramped temperature 52
About Columns 53
Selecting the correct packed glass column type 53
About the column modes 53
Select a column mode 54
Setting the column parameters for constant flow or constant
pressure 55
Enter a flow or pressure program (optional) 55
Programming column pressure or flow 56
Advantages of the optional Backflush Wizard 56
Procedures for manually creating a backflush method 57
Nickel Catalyst Tube 61
About the nickel catalyst tube 61
Nickel catalyst gas flows 61
Setting temperatures for the nickel catalyst tube 62
Advanced User Guide 5
Hydrogen Sensor 63
Instrument logs 63
Calibration 63
Status information 63
Operation with an Agilent data system 64
5 Detectors
About Makeup Gas 66
About the FID 67
How FID units are displayed in Agilent data systems and on the GC 68
To light the FID flame 68
To extinguish the FID flame 68
FID automatic reignition (Lit offset) 68
Recommended starting conditions for new FID methods 69
Setting parameters for FID 70
About the TCD 71
TCD pneumatics 73
TCD carrier, reference, and makeup gas 73
TCD gas pressures 74
Selecting reference and makeup flows for the TCD 75
Chemically active compounds reduce TCD filament life 75
Changing the TCD polarity during a run 76
Detecting hydrogen with the TCD using helium carrier gas 76
Setting parameters for the TCD 76
About the µECD 79
µECD safety and regulatory information 79
µECD warnings 80
µECD gas flows 82
µECD linearity 82
µECD detector gas 82
µECD temperature 83
µECD analog output 83
Recommended starting conditions for new µECD methods 83
µECD makeup gas notes 83
µECD temperature programming 84
Setting parameters for the µECD 84
About the NPD 85
NPD flows and general information 85
NPD flow, temperature, and bead recommendations 86
NPD required gas purity 87
Setting parameters for the NPD 88
Selecting an NPD bead type 89
6 Advanced User Guide
Selecting an NPD jet 90
To configure the NPD 91
Automatically adjusting NPD bead voltage 92
Setting NPD adjust offset on the clock table 93
Aborting NPD adjust offset 93
Extending the NPD bead life 93
Setting the initial bead voltage for new beads 94
Setting NPD bead voltage manually (optional) 94
About the FPD+96
FPD+linearity 97
FPD+Lit Offset 97
FPD+photomultiplier protection 97
FPD+optical filters 98
Inlet liners for use with the FPD+98
FPD+temperature considerations 98
FPD+gas purity 99
FPD+gas flows 99
Lighting the FPD+flame 99
Setting parameters for the FPD+100
About the FPD 102
FPD linearity 103
FPD Lit Offset 103
Starting Up and Shutting Down the FPD 103
FPD photomultiplier protection 103
FPD optical filters 103
Inlet liners for use with the FPD 104
FPD temperature considerations 104
FPD gas purity 104
FPD gas flows 104
Lighting the FPD flame 105
Setting parameters for the FPD 106
6 Valves
The Valve Box 110
Heating the valves 110
Valve temperature programming 110
Valve Control 111
The valve drivers 111
The internal valve drivers 111
Valve Types 113
Configuring a Valve 114
Advanced User Guide 7
Controlling a Valve 115
From the keyboard 115
From the run or clock time tables 115
Gas sampling valve 115
7 GC Output Signals
About Signals 118
Analog Signals 119
Analog zero 119
Analog range 119
Analog data rates 120
Selecting fast peaks (analog output) 121
Digital Signals 122
Digital zero 122
Signal Freeze and Resume 122
Data rates with Agilent data systems 123
Zero Init Data Files 125
8 Auxiliary Devices
About Pressure Control 128
Pressure units 128
8 Advanced User Guide
9
Agilent 7820A Gas Chromatograph
Advanced User Guide
Agilent Technologies
1
Software Keypad
10 Advanced User Guide
1Software Keypad
Using the Software Keypad
The Agilent software keypad (remote controller) provides the
ability to program and use the 7820A Gas Chromatograph (GC).
Refer to the Operating Guide for instructions for its installation
and use.
All instructions in this manual assume the use of the software
keypad unless otherwise noted.
Figure 1 Software keypad (remote controller)
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