Agilent Technologies 708-DS Manuale utente

Agilent Technologies

708-DS

Dissolution Apparatus

Operator’s Manual

708-DS Operator’s Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

70-9058

Edition

Rev E, February 2016

Agilent Technologies, Inc.

3501 Stevens Creek Blvd.

Santa Clara, CA 95052 USA

Warranty

The material contained in this doc-

ument is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further,

to the maximum extent permitted

by applicable law, Agilent disclaims

all warranties, either express or

implied, with regard to this manual

and any information contained

herein, including but not limited to

the implied warranties of mer-

chantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or

performance of this document or of

any information contained herein.

Should Agilent and the user have a

separate written agreement with

warranty terms covering the mate-

rial in this document that conflict

with these terms, the warranty

terms in the separate agreement

shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

U.S. Government Restricted Rights. Soft-

ware and technical data rights granted to

the federal government include only those

rights customarily provided to end user

customers. Agilent provides this custom-

ary commercial license in Software and

technical data pursuant to FAR 12.211

(Technical Data) and 12.212 (Computer

Software) and, for the Department of

Defense, DFARS 252.227-7015 (Techni-

cal Data - Commercial Items) and DFARS

227.7202-3 (Rights in Commercial Com-

puter Software or Computer Software

Documentation).

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in damage to the product or loss

of important data. Do not proceed

beyond a CAUTION notice until

the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the

indicated conditions are fully

understood and met.

708-DS Operator’s Manual 3

Contents

Figures 7

1Safety 11

Electrical Hazards 12

Warning 13

Caution 13

Note 13

Information Symbols 14

2 Introduction 15

Conventions Used in this Manual 17

Serial Number Format 18

3 Setting Up the 708-DS 19

Initial Setup 20

Unpacking Procedure 20

Environmental Requirements for Installation 22

Clearance 22

Equipment, Parts, and Accessories As Shipped 23

Parts and Accessories 23

Tubing / Cable Connections 24

708-DS Heater / Circulator Setup 24

Instrument Level / Water Bath Setup 25

Level Instrument 25

Bath Temperature Probe Installation 28

Handheld Probe Installation 29

4 708-DS Operator’s Manual

Contents

Power Cord Connections 29

708-DS Initial Power Up 29

Filling the Water Bath 30

Level Instrument - Re-verification 31

Heater / Circulator Power-up 31

Agilent 708-DS Setup 32

Vessel Installation 32

Sample Manifold Installation 32

Accessory Installation 36

Setting Basket (Apparatus 1) Heights 42

Setting Paddle (Apparatus 2) Heights 43

4 Operating the 708-DS 45

Main Screen - Options 46

Main Screen - Display Parameters 46

Main Screen - Sample Temperatures 47

Main Screen - Run 48

Main Screen - Stop 55

Main Screen - Drive Unit Up / Down 58

Manual Drive Unit Up / Down 58

Manual Sampling 59

Main Screen - Manifold Up / Down 60

Main Screen - Lock 61

Main Screen - Unlock 62

Main Screen - Remote Control 63

Main Screen - Alarms 64

Main Screen - Maintenance Due Icon 64

Menu Screen - System Menu 65

Menu Screen - Method Editor 66

Menu Screen - Reports 75

Menu Screen - Alarms 78

Menu Screen - Instrument 79

Contents

708-DS Operator’s Manual 5

Menu Screen - Calibration 84

Menu Screen - Diagnostics 87

Menu Screen - User Access 90

General 708-DS Conventions 91

Alphanumeric Data Entry 91

Numeric and Time / Date Entry 92

Parameter Limits / Ranges 93

Agilent 708-DS Notifications 95

Main Screen - Error Conditions 95

Dialog Screens (Green / Blue) 97

Warning Screens (Yellow) 99

Error Screens (Red) 103

5 Maintenance and Troubleshooting 107

Preventive Maintenance 108

Weekly Maintenance 108

Monthly Maintenance 108

Bi-Annual Maintenance 108

Sample Line / Paddle / Basket Care 109

Shafts 109

Baskets 110

Rinsing Sample Lines 111

Rinse Cups (Optional) 112

Vessels and Evaporation Covers 113

Water Bath and Temperature Probes 113

Water Bath Care 113

Water Bath Temperature Probe Accuracy Test 114

Removing or Adjusting Cannulas / Probes 116

Manifold Maintenance 116

Removing the Manifold 116

6 708-DS Operator’s Manual

Contents

Accessing the Top Cover 117

Removing Top Cover 117

Replacing the Top Cover 117

Printer Maintenance 118

Removing a Thermal Paper Roll 118

Inserting a Thermal Paper Roll (5095-0307) 121

Thermal Printer Test 124

Obtaining Warranty and Other Services 124

708-DS Operator’s Manual 7

Figures

Figure 1. Unpacking 20

Figure 2. Removing the Apparatus 21

Figure 3. BATH HEATER Connector 24

Figure 4. Levelers and Stability Feet 25

Figure 5. Level-Adjustment Screw Caps 26

Figure 6. Raising the Stability Feet 27

Figure 7. BATH TEMP Connector 28

Figure 8. Positioning the Temperature Probe 28

Figure 9. Filling the Water Bath 30

Figure 10. Positioning the Manifold for Installation 33

Figure 11. Connecting AutoTemp 34

Figure 12. Affixing the Fasteners 35

Figure 13. Proper Sample Tubing Position 36

Figure 14. Installing Evaporation Covers on Shafts 37

Figure 15. Shaft Locking Collars 37

Figure 16. Dosage Delivery Module and Alignment Post 38

Figure 17. Inserting DDM into DDM Alignment Shaft 39

Figure 18. Attaching DDM to Alignment Post 40

Figure 19. Accessory Installation 41

Figure 20. Tightening the Shaft Locking Collar 42

Figure 21. Inserting Height Spheres 43

Figure 22. Main Screen - Display Parameters 46

Figure 23. Sample Temperatures 47

Figure 24. Select Start Type 48

Figure 25. Select Method 49

Figure 26. Start Options 50

Figure 27. Manual Operation 52

Figure 28. Data Entry 53

Figure 29. Main Screen - Stop 55

8 708-DS Operator’s Manual

Figures

Figure 30. Pause Method 55

Figure 31. Method Paused 56

Figure 32. Pause Duration Alarm 57

Figure 33. Manual Lift Knob 58

Figure 34. Taking a Manual Sample 59

Figure 35. Agilent 708-DS Standard Evaporation Cover 60

Figure 36. Lock the Instrument 61

Figure 37. Unlock the Instrument 62

Figure 38. Remote Control 63

Figure 39. Alarm Time Expired 64

Figure 40. System Menu 65

Figure 41. Method Editor 66

Figure 42. Method Properties Screen 1 67

Figure 43. Method Properties Screen 2 68

Figure 44. Method Properties Screen 3 70

Figure 45. Method Properties Screen 4 72

Figure 46. Timepoint Properties 72

Figure 47. Are You Sure? 74

Figure 48. Reports 75

Figure 49. Select Method to Print 76

Figure 50. Reports 77

Figure 51. Alarms 78

Figure 52. Menu Screen - Instrument Settings Screen 1 79

Figure 53. Menu Screen - Instrument Settings Screen 2 81

Figure 54. Menu Screen - Instrument Settings Screen 3 82

Figure 55. Menu Screen - Instrument Settings Screen 4 83

Figure 56. Paddles/Baskets Sampling Depth 84

Figure 57. Regulatory Calibration Date 86

Figure 58. Diagnostics Screen 1 87

Figure 59. Menu Screen - Diagnostics Screen 2 89

Figure 60. User Level Settings 90

Figure 61. Data Entry 91

Figure 62. Time / Date Entry 92

708-DS Operator’s Manual 9

Figures

Figure 63. Main Screen with Red Error Conditions 95

Figure 64. Rinse Cup 112

Figure 65. Resistance Value of Temperature Probe 115

Figure 66. Near-empty Paper Roll 118

Figure 67. Accessing the Printer Handle 119

Figure 68. Open Printer Chamber 119

Figure 69. Removing the Thermal Paper Roll 120

Figure 70. Inserting a Thermal New Paper Roll 121

Figure 71. Leading Paper and Closing the Lid 122

Figure 72. Closing the Printer Chamber 122

Figure 73. Feeding Paper 123

Figure 74. Printer Test 124

10 708-DS Operator’s Manual

Figures

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