Agilent Technologies 1290 Infinity II Manuale utente

Agilent Technologies

Agilent InfinityLab LC Series

1290 Infinity II

High Speed Pump

User Manual

1290 Infinity II High Speed Pump User Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

G7120-90001 Rev. C

Edition

10/2018

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connection

with the furnishing, use, or perfor-

mance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a

license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of

a U.S. Government prime contract or sub-

contract, Software is delivered and licensed

as “Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in

FAR 2.101(a) or as “Restricted computer

software” as defined in FAR 52.227-19

(June 1987) or any equivalent agency regu-

lation or contract clause. Use, duplication

or disclosure of Software is subject to Agi-

lent Technologies’ standard commercial

license terms, and non-DOD Departments

and Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION

notice until the indicated condi-

tions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indi-

cated conditions are fully

understood and met.

1290 Infinity II High Speed Pump User Manual 3

In This Guide…

This manual covers the Agilent 1290 Infinity II High Speed Pump (G7120A).

1Introduction

This chapter gives an introduction to the pump and an instrument overview.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical

and performance specifications.

3UsingthePump

This chapter explains the operational parameters of the Agilent 1290 Infinity

II High Speed Pump.

4 Optimizing Performance

This chapter gives hints on how to optimize the performance or use additional

devices.

5 Troubleshooting and Diagnostics

Overview about the troubleshooting and diagnostic features.

6 Error Information

This chapter describes the meaning of error messages, and provides

information on probable causes and suggested actions how to recover from

error conditions.

7 Maintenance

This chapter describes the maintenance of the High Speed Pump.

8 Parts and Materials for Maintenance

This chapter provides information on parts for maintenance.

4 1290 Infinity II High Speed Pump User Manual

In This Guide…

9 Identifying Cables

This chapter provides information on cables used with the modules.

10 Hardware Information

This chapter describes the pump in more detail on hardware and electronics.

11 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

12 Appendix

This chapter provides addition information on safety, legal and web.

1290 Infinity II High Speed Pump User Manual 5

Contents

1Introduction 9

Product Description 10

Pump Principle 11

Leak and Waste Handling 13

2 Site Requirements and Specifications 19

Site Requirements 20

Physical Specifications 23

Performance Specifications 24

3UsingthePump 27

Magnets 28

Turn on/off 29

Status Indicators 31

Best Practices 32

Purging the Pump 35

Solvent Information 37

Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260

Infinity II Flexible Pumps 44

Algae Growth in HPLC Systems 49

Setting up the Pump with the Instrument Control Interface 50

Agilent Local Control Modules 60

4 Optimizing Performance 63

Delay Volume and Extra-Column Volume 64

How to Configure the Optimum Delay Volume 65

How to Achieve Higher Resolution 67

Using Solvent Calibration Tables 70

6 1290 Infinity II High Speed Pump User Manual

Contents

5 Troubleshooting and Diagnostics 71

User Interfaces 72

Agilent Lab Advisor Software 73

Pump Leak Rate Test 74

System Pressure Test 79

6 Error Information 81

What Are Error Messages 83

General Error Messages 84

Pump Error Messages 94

7 Maintenance 111

Introduction to Maintenance 112

Warnings and Cautions 114

Overview of Maintenance 116

Cleaning the Module 117

Install Fittings and Capillaries 118

Remove and Install Doors 119

Replace the Shutoff Valve Panel 121

Replace the Pressure Sensor 123

Replace the Solvent Selection Valve (SSV) 125

Change Configuration or Replace the Jet Weaver 127

Replace the Seal Wash Pump 130

Replace the Inlet Valve 131

Release a Stuck Inlet Valve 133

Remove the Pump Head Assembly 135

Pump Head Maintenance (Tool Free) 138

Install the Pump Head Assembly 153

Replace the Outlet Valve 155

Replace the Purge Valve Head 157

Replace Parts of the High Pressure Filter Assembly 160

Replace the Module Firmware 162

Prepare the Pump Module for Transport 163

1290 Infinity II High Speed Pump User Manual 7

Contents

8 Parts and Materials for Maintenance 167

Overview of Maintenance Parts 168

Flow Connections 170

Pump Heads 172

Purge Valve 177

Cover Parts 178

Accessory Kit 179

HPLC System Tool Kit 180

9 Identifying Cables 181

Cable Overview 182

Analog Cables 184

Remote Cables 186

CAN/LAN Cables 190

Agilent Module to PC 191

USB 192

10 Hardware Information 193

Firmware Description 194

Electrical Connections 197

Interfaces 199

Setting the 8-bit Configuration Switch 204

Early Maintenance Feedback 208

Instrument Layout 209

11 LAN Configuration 211

What You Have to Do First 212

TCP/IP parameter configuration 213

Configuration Switch 214

Initialization mode selection 215

Dynamic Host Configuration Protocol (DHCP) 217

Link configuration selection 220

Manual Configuration 221

PC and User Interface Software Setup Setup 226

8 1290 Infinity II High Speed Pump User Manual

Contents

12 Appendix 229

General Safety Information 230

Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) 236

Radio Interference 237

Sound Emission 238

Agilent Technologies on Internet 239

1290 Infinity II High Speed Pump User Manual

Agilent Technologies

Introduction

Product Description 10

Pump Principle 11

Leak and Waste Handling 13

Leak Sensor 16

Waste Concept 17

This chapter gives an introduction to the pump and an instrument overview.

10 1290 Infinity II High Speed Pump User Manual

Introduction

Product Description

The Agilent 1290 Infinity II High Speed Pump can enhance your efficiency

through high speed and chromatographic performance.

A low-delay-volume mixer allows you to run fast gradients for narrow-bore

applications for high laboratory efficiency.

The new 1290 Infinity II LC power range has a high instrument efficiency,

allowing you to run any HPLC and UHPLC method.

The full ISET range enables you to transfer existing methods from different

instruments, including current Agilent systems as well as instruments from

other manufacturers.

Active damping, automatic purge valve, new ultralow dispersion kits or low

delay-volume capability, combine to achieve high instrument and analytical

efficiency.

Figure 1 Overview of the High Speed Pump

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/HDNGUDLQ

3RZHUVZLWFK

3UHVVXUHVHQVRU

3XPSKHDG%

3XPSKHDG$

6HDOZDVKSXPS

-HWZHDYHU

669

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