ALS SEC2020 Manuale utente

Document Version: 2.5.0

Last Revision:July, 2019

SEC2020 SPECTROMETER SYSTEM

USER’S GUIDE

- DEVICE -

Device User’s Guide Contents

https://www.als-japan.com/ 2

Contents

SEC2020

Spectrometer system

.........................................................................4

2. General Information.........................................................................................5

2-1 User Updates.................................................................................................. 5

2-2 Technical changes........................................................................................... 5

2-3 Damaged shipment ........................................................................................ 5

2-4 Product warranty ........................................................................................... 5

2-5 Service information........................................................................................ 6

3. System configuration.......................................................................................7

SEC2021 Spectrometer......................................................................................... 8

SEC2022 Deuterium Halogen light source .......................................................... 10

SEC2023 Cuvette holder ..................................................................................... 12

SEC2024 Platform............................................................................................... 13

AC adaptor and Power cable .............................................................................. 13

USB cable ........................................................................................................... 13

Collimator........................................................................................................... 14

Fiber collimator .................................................................................................. 14

External device connection trigger cable............................................................ 15

Trigger cable....................................................................................................... 15

Plastic cuvette .................................................................................................... 16

SMA905 adaptor for light source........................................................................ 16

SMA905 adaptor for light shielding .................................................................... 16

Hexagon wrench................................................................................................. 16

Software (USB memory)..................................................................................... 17

Quick manual ..................................................................................................... 17

Wavelength Calibration Data Sheet.................................................................... 17

Linearity Test Data Sheet.................................................................................... 17

Waterproof box.................................................................................................. 17

Warranty certificate ........................................................................................... 17

4. Instrument setting for absorbance/transmittance measurement .........18

Example: 1. Using cuvette .................................................................................. 18

Example: 2. Using thin film................................................................................. 19

Example: 3. Using probe..................................................................................... 20

5. Instrument setting for reflectance measurement.....................................22

Device User’s Guide Contents

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Application example using relectance probe...................................................... 22

6. Instrument setting for fluorescence measurement..................................24

Application example using high power LED ........................................................ 24

7. Instrument setting for light source measurement....................................25

Emission intensity measuremen for specific irradiation range measurement..... 25

8. Synchronization with other instruments.....................................................26

9. EU Declarationof Conformity .......................................................................30

10. Contact us .......................................................................................................31

Device User’s Guide 1. SEC2020 Spectrometer system

https://www.als-japan.com/ 4

SEC2020

Spectrometer system

The SEC2020 Spectrometer system is a compact spectrometer system developed by ALS

Co, .Ltd and provided by BAS Inc. One unit can measure a wide wavelength range from

ultraviolet to near infrared (UV/VIS/NIR) with high sensitivity, corresponding to optical

measurements such as spectrum, absorbance, transmittance, reflectance , fluorescence,

light source and concentration.

In addition, BAS, which also provides electrochemical measuring instruments, may also

offer know-how for spectroelectrochemical measurement, electrochemical

measurements combined with spectroscopy.

* Optional products may be prepared separately.

Device User’s Guide 2. General Information

https://www.als-japan.com/ 5

2. General Information

2-1 User Updates

In order to receive any updated information about product, and valuable information

related to current and other ALS products, please register your e-mail address at our

local distributors. We would like to know about your present status and interests

regarding electrochemical analysis.

2-2 Technical changes

We reserve the right to make technical changes to improve the instrument without

notice.

2-3 Damaged shipment

Breakage of any part of this instrument during shipping should be reported

immediately to the freight handler and ALS Customer service.

It is necessary to keep the original packing box and contents for inspection by the

freight forwarder. ALS will replace any new instrument damaged in shipping with an

identical product as expediently as possible after the claim filing date. Claims not filed

within 7 days after shipping may be invalid.

Do not return damaged goods to ALS directly. Please contact with your local

distributor informing them of its damaged status.

They will contact with our service department.

2-4 Product warranty

ALS Co., Ltd warrants equipment manufactured by the company to be free from

defects in material and workmanship for a period of 90 days from the date of

shipment. This assumes normal usage under commonly accepted operating

parameters. ALS agrees to either repair or replace, at its sole option and free of part

charges to the buyer, any parts of such instrumentation which, under proper and

normal conditions of use, prove to be defective within 90 days from date of shipment.

Electrochemical cells and working electrodes are warranted for 30 days.

ALS neither assumes nor authorizes any person to assume for it any other liability in

Device User’s Guide 2. General Information

https://www.als-japan.com/ 6

connection with the sale, installation, service, or use of its instrumentation.

All products manufactured by ALS are tested and inspected prior to shipment. Upon

prompt notification by the buyer, ALS will correct any defects in warranted

equipment by its manufacture either by return of the item to our factory, or

shipment of a repaired or replacement part. ALS will not be obliged, however, to

replace or repair any piece of equipment which has been abused, improperly

installed, altered, damaged or repaired by others. Defects in equipment do not

include decomposition, wear, or damage by chemical action or corrosion.

This instrument is manufactured, either wholly or in part, for research purposes only.

Use in medical diagnosis is not intended, implied or recommended by the

manufacturer. Use for this purpose and accountability for the same rests entirely with

the user.

Limited obligations covered by this warranty include:

In the case of instruments not of ALS manufacture, the original manufacturer’s

warranty applies.

Shipping charges under warranty are covered only in one direction. The buyer is

responsible for shipping charges to the factory, if return of the part is required.

Expendable items including disposable items such as working electrode, reference

electrodes, source lights, panel lights, fuses, etc. are excluded from the warranty

2-5 Service information

ALS provides a skilled service staff to solve your equipment oriented problems. For

further details, please contact us by e-mail (sales@als-japan.com).

Following discussion of your specific difficulties, an appropriate course of action will

be described and the problem resolved accordingly.

Please contact with local distributor and describe to them the problem you are

having in full detail.

They will obtain a RETURN MERCHANDISE AUTHORIZATION NUMBER (RMA#). The

RMA# identifies you as the sender. All correspondence and shipments should be sent

to ALS.

Device User’s Guide 3. System Configuration

https://www.als-japan.com/ 7

3. System configuration

SEC 2020 spectrometer system consists of four basic accessories. It consists of SEC 2021

spectrometer, SEC 2022 deuterium halogen light source, SEC 2023 cuvette holder, and

SEC 2024 platform.

1314

916

Figure 3-1: Configuration and List of accessories

Spectrometerer

Cuvette holder

Light source

Platform

De sc ription Qty

1 SEC20 21 Spectrome te r 1

SEC20 22 Deu te rium halogen light source

3 SEC20 23 Cu vette h older 1

4 SEC20 24 Platform 1

5 AC adapto r 1

6 Power c able 1

7 USB cable 1

8 Collimator 2

9 Fibe r collimator 1

10 Platform sc rew 7

External device conn ection trigge r cable

12 Trigger c able 1

13 Plastic c uvette 1

14 SMA905 adaptor for light sourc e 3

15 SMA905 adaptor for light shielding 2

16 Hexagon wrenc h0.8 9mm 1

17 Hexagon wrenc h1.5 0mm 1

18 Software （USB me mory） 1

(19) Quick manual 1

(20) Wavelen gth Calibration Data Sh eet 1

(21) Lin earity Test Data She et 1

(22) Waterproof box 1

(23) Warran ty certificate 1

Device User’s Guide 3. System Configuration

https://www.als-japan.com/ 8

SEC2021 Spectrometer

SEC2020 Spectrometer system is equipped with SEC 2021 spectrometer as standard

content. With highly functional grating and optical design, it is possible to measure a wide

wavelength range from ultraviolet to near infrared (UV / VIS / NIR) with high sensitivity

with one unit.

Spectrometer specification

Description

SEC2021-025-DUVN

Detector

2048 element linear silicon CCD array

Wavelength range

200 –1025 nm

Grating

Blaze wavelength (300 nm)

Slit

25 μm

Wavelength resolution

1.3 nm

Fiber connector

SMA905 Core diameter: 600 μm NA = 0.22

Interface

USB 2.0

Operating system

Windows TM 7/8.1/10, 32/64 bit

Size (W x D x H)

86 x 110 x 32 mm

Figure 3-2: SEC2021 Spectrometer

Device User’s Guide 3. System Configuration

https://www.als-japan.com/ 9

I/O Port Pin

The Pin number of the I/O port for the spectrometer controlling is showing below:

Pin No.

Signal

Definition

Function

Power

5V Output

When connecting to the PC's USB port, this pin is connected to

VBUS. Up to 100 mA current

No connection

Output

Shutter

Shutter ON/OFF

Output

D2_ON

D2 light source ON/OFF

Output

HAL_ON

Halogen light source ON/OFF

Input

Trigger-IN

TTL

GND

Ground

Figure 3-3: SEC2021 Spectrometer Port Pin number

Device User’s Guide 3. System Configuration

https://www.als-japan.com/ 10

SEC2022 Deuterium Halogen light source

SEC2020 Spectrometer system is equipped with SEC 2022 deuterium halogen light source

as standard content.

Light source specification

Description

SEC2021-025-DUVN

Light type

Deuterium halogen light source

Wavelength range

200 –1700 nm

Stability

< 0.1 %

Drift

< 0.25 % h

Bulb life

> 1000 h (D2 lamp)

> 2000 h (halogen lamp)

Fiber connector

SMA905

Size (W x D x H)

100 x 165 x 46 mm

Figure 3-4: Switch location for the light source

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