ACOEM Serinus 44 Manuale utente
Serinus 44
NO/NO2/NOx/NH3
Analyser
Version 1.0
Ecotech Pty Ltd is now part of the Acoem Group and as such,
the branding of our instruments & software has also changed
to ‘Acoem’.
Over time we will be updating the content of all documents to
reflect the Acoem branding convention.
In the interim, please note that while the cover of this document
features Acoem branding, information contained within its
pages still utilises the original ‘Ecotech’ name.
Serinus 44 User manual 1.0 Front Matter
i
Manufacturers statement
Thank you for selecting the Acoem Serinus 44 NO/NO2/NOX/NH3Analyzer.
The Serinus series is the next generation of Acoem designed and manufactured gas
analyzer, the Serinus 44 will perform NO, NO2, NOX, NH3 measurements over a
range of 0-20ppm with a LDL of 0.4 ppb.
This User Manual provides a complete product description including operating
instructions, calibration, and maintenance requirements for the Serinus 44.
Reference should also be made to the relevant local standards, which should be used
in conjunction with this manual. Some relevant standards are listed in the References
section of this manual.
If, after reading this manual you have any questions or you are still unsure or unclear
on any part of the Serinus 44 then please do not hesitate to contact Acoem or your
local Acoem distributor.
Acoem also welcomes any improvements that you feel would make this a more
useable and helpful product then please send your suggestions to us here at Acoem.
Please help the environment and recycle the
pages of this manual when finished using it.
Notice
The information contained in this manual is subject to change without notice. Acoem
reserves the right to make changes to equipment construction, design, specifications
and /or procedures without notice.
Copyright © 2010 All rights reserved. Reproduction of this manual, in any form,
is prohibited without the written consent of Acoem Pty Ltd.
Front Matter Serinus 44 User manual 1.0
ii
WARNING
Hazardous voltages exist within the analyzer. The analyzer lid should be closed and
quarter turn lid fasteners locked when the analyzer is left unattended or turned on.
Ensure the power cord, plugs and sockets are maintained in a safe working condition.
Safety requirements
To reduce the risk of personal injury caused by electrical shock, follow all
safety notices and warnings in this documentation.
If the equipment is used for purposes not specified by Acoem, the protection
provided by this equipment may be impaired.
Replacement of any part should only be carried out by qualified personnel,
using only parts specified by Acoem as these parts meet stringent Acoem
quality assurance standards. Always disconnect power source before removing
or replacing any components.
Serinus 44 User manual 1.0 Front Matter
iii
Factory service/warranty
This product has been manufactured within an ISO9001/ISO 14001 accredited facility
with care and attention.
The product is subject to a 12-month warranty on parts and labour from date of
shipment (the warranty period). The warranty period commences when the product is
shipped from the factory. Lamps, fuses, batteries and consumable items are not
covered by this warranty.
Each analyzer is subjected to a vigorous testing procedure prior to despatch and will
be accompanied with a parameter list and a multipoint calibration check thereby
enabling the analyzer to be installed and ready for use without any further testing.
To ensure that we process your factory repairs and returned goods efficiently and
expeditiously, we need your help. Before you ship any equipment to our
factory, please call your local Acoem service response centre (or distributor) to
obtain a return authorisation number.
When you contact Acoem please provide the following information:
1. your name, telephone number and facsimile number
2. Your company name
3. The model number or a description of each item
4. The serial number of each item, if applicable
5. A description of the problem or the reason you are returning the equipment
(e.g. sales return, warranty return, calibration, etc)
If you are required to return the equipment, the following documents should also be
sent:
1. Your name, number and facsimile number
2. Your company name with return shipment
3. The model number or a description of each item
4. The serial number of each item, if applicable
A description of the problem/reason you are returning the equipment
Front Matter Serinus 44 User manual 1.0
iv
Claims for Damaged Shipments and
Shipping Discrepancies
Damaged shipments
1. Inspect all instruments thoroughly on receipt. Check materials in the
container(s) against the enclosed packing list. If the contents are damaged
and/or the instrument fails to operate properly, notify the carrier and Acoem
immediately.
2. The following documents are necessary to support claims:
a. Original freight bill and bill lading
b. Original invoice or photocopy of original invoice
c. Copy of packing list
d. Photographs of damaged equipment and container
e. Contact your freight forwarder for insurance claims
You may want to keep a copy of these documents for your records also.
Refer to the instrument name, model number, serial number, sales order
number, and your purchase order number on all claims. Upon receipt of a
claim, we will advice you of the disposition of your equipment for repair or
replacement.
Shipping Discrepancies
Check all containers against the packing list immediately on receipt. If a shortage
or other discrepancy is found, notify the carrier and Acoem immediately. We will not
be responsible for shortages against the packing list unless they are reported
promptly (within 7 days).
Serinus 44 User manual 1.0 Front Matter
v
Internationally recognised symbols used
on Acoem Equipment
Electrical fuse
IEC 60417, No. 5016
Earth (ground) terminal
IEC 417, No. 5017
Equipotentiality
IEC 417, No. 5021
Alternating current
IEC 417, No. 5032
Caution, hot surface
IEC 417, No. 5041
Caution, refer to
accompanying documents
ISO 3864, No. B.3.1
Caution, risk of electric shock
ISO 3864, No. B.3.6
Front Matter Serinus 44 User manual 1.0
vi
Manual Revision History
MAN 0075
M010034
1.0
August2010
Acoem Manual ID:
Manual PN:
Current Revision:
Date released:
Description: User Manual for the Serinus 44 NO/NO2/NOX/NH3
analyzer
This manual is the full user manual for the Serinus 44 NO/NO2/NOX/NH3Analyzer.
This manual contains all relevant information on theory, specifications, installation,
operation, maintenance and calibration. Any information that cannot be found within
this manual can be found by contacting Acoem at:
Email: Help [email protected]
Service [email protected]
Parts [email protected]
Phone: +61 1300 364 946
Fax: +61 1300 668 763
Address: Acoem Australasia
1492 Ferntree Gully Rd
Knoxfield Victoria
Australia 3180
Website www.acoem.com
Edition
Date
Summary
Pages
1.0
August 2010
Initial Release
all
Serinus 44 User manual 1.0 Front Matter
vii
Table of Contents
1INTRODUCTION ............................................................................................................ 1
1.1 DESCRIPTION ................................................................................................................... 1
1.2 SPECIFICATIONS .............................................................................................................. 1
1.2.1 MEASUREMENT ............................................................................................................. 1
1.2.2 PRECISION/ACCURACY .................................................................................................. 1
1.2.3 CALIBRATION ................................................................................................................ 1
1.2.4 POWER ........................................................................................................................... 2
1.2.5 OPERATING CONDITIONS ............................................................................................... 2
1.2.6 COMMUNICATIONS ........................................................................................................ 2
1.2.7 PHYSICAL DIMENSIONS .................................................................................................. 2
1.3 NOMENCLATURE ............................................................................................................. 3
1.4 BACKGROUND/ THEORY ................................................................................................. 4
1.4.1 MEASUREMENT THEORY ............................................................................................... 4
1.4.2 KALMAN FILTER THEORY .............................................................................................. 5
1.5 INSTRUMENT DESCRIPTION ............................................................................................ 5
1.5.1 PARTICULATE FILTER .................................................................................................... 6
1.5.2 DELAY LOOP .................................................................................................................. 6
1.5.3 MOLYCON CONVERTER ................................................................................................. 6
1.5.4 VALVE MANIFOLD ......................................................................................................... 6
1.5.5 SAMPLE VALVE MANIFOLD ........................................................................................... 6
1.5.6 PRESSURE TRANSDUCERS .............................................................................................. 6
1.5.7 HTO 1000N EXTERNAL THERMAL CONVERTER (OPTIONAL) ........................................ 6
1.5.8 OPTICAL CELL ............................................................................................................... 7
1.5.9 MAIN CONTROLLER PCB .............................................................................................. 7
1.5.10 POWER SUPPLY ............................................................................................................ 7
1.5.11 COMMUNICATIONS ...................................................................................................... 8
2INSTALLATION ............................................................................................................. 9
2.1 INITIAL CHECK ................................................................................................................ 9
2.2 MOUNTING/SITING ........................................................................................................ 10
2.3 INSTRUMENT SETUP ...................................................................................................... 10
2.3.1 PNEUMATIC CONNECTIONS .......................................................................................... 11
2.3.2 POWER CONNECTIONS ................................................................................................. 12
2.3.3 COMMUNICATIONS CONNECTIONS .............................................................................. 12
2.3.4 ANALYZER SET UP ....................................................................................................... 13
2.4 TRANSPORTING/STORAGE ............................................................................................ 14
3OPERATION.................................................................................................................. 15
3.1 WARMUP ........................................................................................................................ 15
3.2 GENERAL OPERATIONAL INFORMATION ..................................................................... 15
3.3 MAIN SCREEN ................................................................................................................ 16
3.4 SAMPLING ...................................................................................................................... 18
3.5 MENUS AND SCREENS .................................................................................................... 18
3.5.1 QUICK MENU ............................................................................................................... 19
3.5.2 ANALYZER STATE ....................................................................................................... 20
Front Matter Serinus 44 User manual 1.0
viii
3.5.3 MEASUREMENT SETTINGS ........................................................................................... 23
3.5.4 CALIBRATION MENU .................................................................................................... 24
3.5.5 SERVICE ....................................................................................................................... 26
3.5.6 COMMUNICATIONS ...................................................................................................... 32
4CALIBRATION ............................................................................................................. 35
4.1 ZERO CALIBRATION...................................................................................................... 35
4.2 SPAN CALIBRATION ...................................................................................................... 36
4.3 MULTIPOINT CALIBRATION ......................................................................................... 37
4.4 NO2 CONVERTER EFFICIENCY ..................................................................................... 39
4.5 NH3 CONVERTER EFFICIENCY ..................................................................................... 39
4.6 PRECISION CHECK ......................................................................................................... 40
4.7 PRESSURE CALIBRATION .............................................................................................. 41
5COMMUNICATION ..................................................................................................... 44
5.1 RS232 COMMUNICATION ............................................................................................. 44
5.2 USB COMMUNICATION ................................................................................................. 44
5.3 TCP/IP NETWORK COMMUNICATION ......................................................................... 44
5.4 DIGITAL/ANALOG COMMUNICATION .......................................................................... 46
5.5 SERINUS DOWNLOADER PROGRAM .............................................................................. 49
5.5.1 SETTINGS ..................................................................................................................... 49
5.5.2 DATA ........................................................................................................................... 51
5.5.3 REMOTE SCREEN .......................................................................................................... 52
5.5.4 REMOTE TERMINAL ..................................................................................................... 53
6SERVICE ........................................................................................................................ 54
6.1 PNEUMATIC DIAGRAM .................................................................................................. 54
6.2 MAINTENANCE TOOLS .................................................................................................. 54
6.3 RECOMMENDED MAINTENANCE SCHEDULE ................................................................ 55
6.4 MAINTENANCE PROCEDURES ....................................................................................... 56
6.4.1 PARTICULATE FILTER REPLACEMENT .......................................................................... 56
6.4.2 CLEAN FAN FILTER ...................................................................................................... 57
6.4.3 DFU REPLACEMENT .................................................................................................... 57
6.4.4 SINTERED FILTER REPLACEMENT ................................................................................ 57
6.4.5 QUICK LEAK TEST ........................................................................................................ 58
6.4.6 ADVANCED LEAK CHECK ............................................................................................. 59
6.4.7 REPLACE PMT DESICCANT PACKS............................................................................... 59
6.4.8 CLEAN REACTION CELL ............................................................................................... 60
6.4.9 PRESSURE SENSOR CHECK ........................................................................................... 61
6.5 PARTS LIST ..................................................................................................................... 61
6.6 UPDATING FIRMWARE .................................................................................................. 62
7TROUBLESHOOTING ................................................................................................ 63
7.1 ZERO FLOW ................................................................................................................... 64
7.2 ELECTRONIC ZERO ADJUST.......................................................................................... 64
7.3 NOISY READINGS ........................................................................................................... 65
7.4 CONVERTER TEMPERATURE FAILURE ......................................................................... 65
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