Agilent Technologies G1323B Manuale utente

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Agilent 1200 Series

Handheld Control

Module

User’s Guide

1200 Series Handheld Control Module Users’s Guide

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

into a foreign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Microsoft ® - Microsoft is a U.S. registered

trademark of Microsoft Corporation.

Manual Part Number

G1323-90010

Edition

02/2006

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn, Germany

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or per-

formance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

this document are furnished under a license

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

If software is for use in the performance of a

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

or as a “commercial item” as defined in FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987) or any equivalent agency regulation or

contract clause. Use, duplication or disclo-

sure of Software is subject to Agilent Tech-

nologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receive no greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a haz-

ard. It calls attention to an operat-

ing procedure, practice, or the like

that, if not correctly performed or

adhered to, could result in damage

to the product or loss of important

data. Do not proceed beyond a

CAUTION notice until the indicated

conditions are fully understood and

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in personal injury or death. Do not

proceed beyond a WARNING

notice until the indicated condi-

tions are fully understood and

met.

1200 Series Handheld Control Module Users’s Guide 3

In This Guide…

This book describes how to operate the Agilent 1200 Series modules and

systems for HPLC using the control module.

Solvent cabinet

Vacuum degasser

Pump

Column compartment

Autosampler

Detector

Control module

4 1200 Series Handheld Control Module Users’s Guide

The control module provides complete local control and monitoring of a single

module or an entire Agilent 1200 Series system. There is no data evaluation in

the control module. The control module allows you to do a variety of HPLC

tasks including automated sample preparation and injection, isocratic,

gradient and multiple method analyses.

Chapter Overview

Part 1 Using the Agilent 1200 Series Control Module

This part describes the control mode, its features and its functionality.

1 The Agilent 1200 Series Control Module

This chapter gives an overview over the Agilent 1200 Series control module.

2 Working with the Control Module

This chapter describes how to use the Agilent 1200 Series control module.

Part 2 Using the Agilent 1200 Series Modules

This part describes how to use the individual HPLC modules to run isocratic,

gradient and multiple-vial analyses using a single method or more than one

method.

3UsingthePump

This chapter contains operational details for the Agilent 1200 Series pumping

systems.

4UsingtheDegasser

This chapter contains operational details for the Agilent 1200 Series vacuum

degasser.

5 Using the Autosampler

This chapter contains operational details for the Agilent 1200 Series

autosampler.

1200 Series Handheld Control Module Users’s Guide 5

6 Using the Manual Injection Valve

This chapter contains operational details for the Agilent 1200 Series manual

injection valve.

7 Using the Detectors

This chapter contains operational details for the Agilent 1200 Series variable

wavelength, multiple wavelength, refractive index, fluorescence light, and

diode array detectors.

8 Using the Column Compartment

This chapter contains operational details for the Agilent 1200 Series

thermostatted column compartment.

Part 3 Using the Agilent 1200 Series LC System With Control Module

This part describes how to run isocratic, gradient and multiple-vial analyses

using a single method or more than one method.

9 Running an Isocratic Analysis

This chapter describes how to analyze the Agilent Technologies isocratic

standard sample using a single injection analysis.

10 Running a Gradient Analysis

This chapter describes how to analyze the Agilent Technologies isocratic

standard sample using a gradient analysis.

11 Running Multiple-Vial Analyses

This chapter descibes how to setup multiple vial analyses using the same

method and different methods.

12 Running an Injector Program

This chapter descibes how to create an injector program.

13 Maintaining the Control Module

This chapter shows the repair items.

6 1200 Series Handheld Control Module Users’s Guide

A Appendix

This chapter contains safety information.

Related Documents

Each HPLC module is supplied with a Reference Manual or User Manual.

The control module is supplied with the following:

• User’s Guide

• Software Overview Guide

1200 Series Handheld Control Module Users’s Guide 7

Contents

1 The Agilent 1200 Series Control Module 15

Control Module Features 16

Control Module Keys 17

The i (info) key - Online Information System 19

The m (menu) key 20

The Esc key 20

The Enter key 21

Navigation keys 21

Action keys 21

Selection keys 21

Direction keys 21

Numeric/Alphanumeric keys 22

Control Module Software 23

The Control Module User Interface 23

Analysis Screen 23

System Screen 27

Status Screen 29

Samples Screen 30

Plot Screen 31

Control Module Versions 32

2 Working with the Control Module 35

Installing the Control Module 36

General Functions 37

Turning On/Off LC System and Modules 37

Setting Date and Time 37

8 1200 Series Handheld Control Module Users’s Guide

Contents

Setting Display Contrast 37

Adjusting View 38

Configuring the LC System 38

Troubleshooting 39

Troubleshooting the Control Module 39

Inserting and Removing PC cards 40

Working with Methods 41

Loading a Method 41

Modifying a Method 42

Specifying a Method Name 42

Protecting a Method 43

Saving a Method 44

Deleting a Method 45

Exchanging Methods With the PC Card 45

Transferring Methods Between LC Systems 46

Time Programming 47

Automating Analyses 48

Displaying Data Graphically 50

Selecting Signals 50

Rescaling the Plot Screen 51

Toggling Signals 52

Displaying Exact Signal Values 52

Print Graph 52

Logbooks 53

Maintenance Logbook 53

Error Logbook 54

System Logbook 54

EMF (Early Maintenance Feedback) 54

Printing Screens 55

Print Plot 55

Contents

1200 Series Handheld Control Module Users’s Guide 9

Print Logbooks 56

Print Method 56

Print Timetable 56

Print Sequence 56

Print Injector Program 56

Connecting External Devices 57

APG Remote 57

GPIB 59

Serial / RS-232 59

MIO 59

BCD 59

External Contacts 59

Firmware Updates 60

Coexecution with Agilent ChemStation 61

Features 61

Restrictions 62

3UsingthePump63

Turning the Pump On and Off 64

Entering Settings 64

Purging the Pump 64

Purging Procedure 65

Adjusting Compressibility 66

Adjusting Stroke Volume 68

Automatic Shut-down 68

Troubleshooting the Pump 68

Tracking Pump History / Pump EMF Limits 69

Resetting the Pump 70

10 1200 Series Handheld Control Module Users’s Guide

Contents

Resetting the Pump Settings 70

4UsingtheDegasser71

Starting the Degasser 72

Removing Gas Bubbles 72

Changing Solvents 73

5 Using the Autosampler 75

Configuring the Autosampler 76

Configuring Interfaces 76

Entering Settings 77

Setting the Injection Mode 77

Optimizing Autosampler Performance 78

Setting up the Thermostatted Autosampler 79

Aligning Transport Arm/Gripper 80

Tracking Autosampler History / EMF limits 81

Resetting the Autosampler 81

Reset to Default Settings 81

Troubleshooting the Autosampler 82

6 Using the Manual Injection Valve 83

About the Injection Valve 84

Making An Injection 85

Completely Filling the Sample Loop 85

Partially Filling the Sample Loop 86

How Much Sample Is Actually Injected? 86

How Much Sample Do I Need? 87

An Alternative Way to Fill The Loop 87

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