Agilent Technologies G1157A Manuale utente

Agilent Technologies

Agilent 1200 Series

Valves

User Manual

Agilent 1200 Series Valves

Notices

No part of this manual may be reproduced in

any form or by any means (including elec-

tronic storage and retrieval or translation

intoaforeign language) without prior agree-

ment and written consent from Agilent

Technologies, Inc. as governed by United

States and international copyright laws.

Manual Part Number

G1156-90010

Edition

02/06

Printed in Germany

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn, Germany

Warranty

The material contained in this docu-

ment is provided “as is,” and is sub-

ject to being changed, without notice,

in future editions. Further, to the max-

imum extent permitted by applicable

law, Agilent disclaims all warranties,

either express or implied, with regard

to this manual and any information

contained herein, including but not

limited to the implied warranties of

merchantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or per-

formance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty

terms covering the material in this

document that conflict with these

terms, the warranty terms in the sep-

arate agreement shall control.

Technology Licenses

The hardware and/or software described in

thisdocumentarefurnishedunder alicense

and may be used or copied only in accor-

dance with the terms of such license.

Restricted Rights Legend

Ifsoftwareis foruseinthe performance ofa

U.S. Government prime contract or subcon-

tract, Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June 1995),

orasa “commercialitem” asdefinedin FAR

2.101(a) or as “Restricted computer soft-

ware” as defined in FAR 52.227-19 (June

1987)oranyequivalentagencyregulationor

contract clause. Use, duplication or disclo-

sure of Software is subject to Agilent Tech-

nologies’ standard commercial license

terms, and non-DOD Departments and

Agencies of the U.S. Government will

receiveno greater than RestrictedRights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will receive

no greater than Limited Rights as defined in

FAR 52.227-14 (June 1987) or DFAR

252.227-7015 (b)(2) (November 1995), as

applicable in any technical data.

Safety Notices

CAUTION

A CAUTION notice denotes a haz-

ard. It calls attention to an operat-

ing procedure, practice, or the like

that, if not correctly performed or

adhered to, could result in damage

to the product or loss of important

data. Do not proceed beyond a

CAUTIONnoticeuntiltheindicated

conditionsarefullyunderstoodand

met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adheredto, could result

in personal injury or death. Do not

proceed beyond a WARNING

notice until the indicated condi-

tions are fully understood and

met.

Agilent 1200 Series Valves 3

In This Guide…

The Agilent 1200 Series valves provide the user a

comprehensive solutions for more flexibility through solvent

selection and column selection. They offer new automation

capabilities for sample preparation as well as higher sample

throughput with alternating column regeneration. The Agilent

1200 Series valves are fully integrated in the CAN environment

(control area network) of the Agilent 1200 Series LC system and

can be controlled by the Agilent ChemStation Software. The

following types of valves will be described in this manual:

•G1157A Agilent 1200 Series 2 Position/10 Port Valve

•G1158A Agilent 1200 Series 2 Position/ 6 Port Valve

•G1159A Agilent 1200 Series 6 Position Selection Valve

•G1160A Agilent 1200 Series 12 Position/13 Port Selection

Valve

•G1162A Agilent 1200 Series 2 Position/ 6 Port Micro Valve

•G1163A Agilent 1200 Series 2 Position/10 Port Micro Valve

These valves and the corresponding capillary kits for

alternating column regeneration, sample enrichment, sample

clean-up, column selection or solvent selection will allow you to

implement these applications easily.

Chapter 1, “Installation and Configuration,” starting on page 7

will describe how to install and configure the Agilent 1200

Series valves.

Chapter 2, “Operation,” starting on page 17 will describe the

Agilent ChemStation valve interface and how to setup the

valves in your analytical method.

Chapter 3, “Maintenance, Repair, and Troubleshooting,”

starting on page 25 will describe recommended maintenance

and repair procedures as well as troubleshooting tools.

4Agilent 1200 Series Valves

Chapter 4, “Valve Applications,” starting on page 39 will

describe common application, e.g. alternating column

regeneration, and how to setup your valves for these

applications.

contents

Agilent 1200 Series Valves 5

Contents

1 Installation and Configuration

Site Requirements 8

Unpacking the Agilent 1200 Series valve 9

Damaged Packaging 9

Delivery Checklist 9

Hardware Installation 12

Setting up the CAN connection 13

Settingup thepowerconnectiontootherAgilent1200 SeriesLC

modules 13

Setting up the power connection to the external power

supply 13

Software Configuration 14

2Operation

Operating the Valve using Agilent ChemStation 18

Handheld Controller functions 22

3 Maintenance, Repair, and Troubleshooting

Status Indicators 26

Maintenance and Repair 27

Replacing the stator face and the rotor seal for standard valves

(G1157A, G1158A, G1159A, G1160A) 28

Replacing the rotor seal for micro valves (G1162A and

G1163A) 30

Early Maintenance Feedback (EMF) 32

System Errors and Troubleshooting 34

System Errors 34

Valve Synchronization 37

6Agilent 1200 Series Valves

contents

4 Valve Applications

Alternating Column Regeneration 40

Sample enrichment and Sample stripping 44

Sample enrichment 44

Sample stripping 45

Column Selection 48

Solvent Selection 50

5Parts General Parts 54

Capillaries and Fittings for analytical and preparative flow

rates 56

Capillaries and Fittings for micro valves 57

6 Specifications

7 Safety Information

General Safety Information 66

Lithium Batteries Information 69

Radio Interference 70

Sound Emission 71

Solvent Information 72

Agilent Technologies on Internet 73

Index 75

Agilent 1200 Agilent 1200 Series Valves

User Manual

Agilent Technologies

Installation and Configuration

Site Requirements 8

Unpacking the Agilent 1200 Series valve 9

Hardware Installation 12

Software Configuration 14

8Agilent 1200 Series Valves

1 Installation and Configuration Site Requirements

Site Requirements

The requirements for the Agilent 1200 Series Valves are displayed Table 1 and

Table 2 on page 8. The 24 Volts DC power can be supplied by an external

power supply (0950-4422) or by one of the following Agilent 1200 Series LC

modules with DC CAN adapter.

•Agilent 1200 Series preparative pump (G1361A)

•Agilent 1200 Series fraction collectors (G1364A, G1364B, G1364C, G1364D)

•Agilent 1200 Series high performance autosampler(G1367B)

•Agilent 1200 Series micro well-plate autosampler (G1377A)

•Agilent 1200 Series dual-loop autosampler PS (G2258A)

Table 1 Site Requirements for Agilent 1200 Series Valves

Type Specification

•Weight 1.9 Kg (4.2 lbs)

•Dimensions

•(height x width x depth) 92 x 84 x 200 mm

(9.2 x 3.3 x 8.0 inches)

•Power supply 24 Volts DC (1.7 amps)

•Ambient operating temperature 4 to 55°C (39 to 131°F)

•Humidity < 95%, non-condensing

•Safety Standards IEC, CSA, UL, EN

Installation category II,

pollution degree 2

For indoor use only

Table 2 System Requirements

Revision

•Agilent 1200 Firmware A.05.04 and higher

•Control Module Firmware G1323B B.03.11 and higher

•Agilent ChemStation Software A.09.03 and higher

Agilent 1200 Series Valves 9

Installation and Configuration 1

Unpacking the Agilent 1200 Series valve

Damaged Packaging

If the delivery packaging shows signs of external damage, please call your

Agilent Technologies sales and service office immediately. Inform your service

representative that the Agilent 1200 Series valve may have been damaged

during shipment.

Delivery Checklist

Ensure all parts and materials have been delivered with the Agilent 1200

Series valve. The delivery checklists are displayed in Table 3 (for G1157A,

G1158A, G1159A, G1160A) and in Table 4 (for G1162A, G1163A). Please

report missing or damaged parts to your Agilent Technologies sales and

service office.

CAUTION If there are signs of damage, please do not attempt to install the valve.

Table 3 Delivery checklist for Agilent 1200 Series valves G1157A, G1158A, G1159A and

G1160A

Quantity Description Part Number

1 Agilent 1200 Series Valve

1 Declaration of conformity

1 Rail assembly for Column Organizer

1 Accessory kit containing

1•CAN Cable, 1m long 5181-1519

1•DC-CAN cable 5181-1533

10 •Fitting Screw long 5065-4454

12 •Fitting Screw extra long 5065-9967 (10/pk)

10 Agilent 1200 Series Valves

1 Installation and Configuration Unpacking the Agilent 1200 Series valve

The M4 micro valve fittings support the Agilent PEEK coated fused silica

capillaries (O.D. 0.8mm or 1/32”). The M4 micro valve plug is supplied for

pressure (leak) testing.

1•Hex Key 9/64” T-handle 8710-2394

1•Hex Key 3/32”

1•wrench 8710-0510

1•socket wrench (Rheotool) 1/4 8710-2391

Table 4 Delivery checklist for Agilent 1200 Series micro valves G1162A and G1163A

Quantity Description Part Number

1 Agilent 1200 Series Micro Valve

1 Declaration of conformity

1 Rail assembly for Column Organizer 5065-4450

6/10 M4 micro valve fittings 5065-4410*

* The consumable kit 5065-4410 contains six M4 micro valve fittings.

1 M4 micro valve plug 5065-4410†

† The consumable kit 5065-4410 contains two M4 micro valve plugs.

1 Accessory kit containing

1•CAN Cable, 1m long 5181-1519

1•DC-CAN cable 5181-1533

1•Hex Key 9/64” T-handle 8710-2394

1•Hex Key 3/32”

1•wrench 8710-0510

1•socket wrench (Rheotool) 1/4 8710-2391

Table 3 Delivery checklist for Agilent 1200 Series valves G1157A, G1158A, G1159A and

G1160A (continued)

Quantity Description Part Number

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